Grain Size Altering Yielding Mechanisms in Ultrafine Grained High-Mn Austenitic Steel: Advanced TEM Investigations

Chang-Yu Hung, Y. Bai, N. Tsuji, M. Murayama
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引用次数: 25

Abstract

Abstract The underlying mechanism of discontinuous yielding behavior in an ultrafine-grained (UFG) Fe-31Mn-3Al-3Si (wt.%) austenitic TWIP steel was investigated by the use of advanced TEM technique with taking the plastic deformation mechanisms and their correlation with grains size near the macroscopic yield point into account. Typical yield drop mechanisms such as the dislocation locking by the Cottrell atmosphere due to the presence of interstitial impurities cannot explain the origin of this phenomenon in the UFG high-Mn austenitic TWIP steel. Here, we experimentally revealed that the plastic deformation mechanisms in the early stage of deformation, around the macroscopic yield point, show an obvious association with grain size. More specifically, the main mechanism shifts from the conventional slip in grain interior to twinning nucleated from grain boundaries with decreasing the grain size down to less than 1 μm. Our observation indicates that the grain size dependent deformation mechanisms transition is also deeply associated with the discontinuous yielding behavior as it could govern the changes in the grain interior dislocation density of mobile dislocations around the macroscopic yield point.
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超细晶高锰奥氏体钢晶粒尺寸改变屈服机制:先进的透射电镜研究
摘要采用先进的透射电镜技术研究了超细晶(UFG) Fe-31Mn-3Al-3Si (wt.%)奥氏体TWIP钢的不连续屈服行为的潜在机制,并考虑了宏观屈服点附近的塑性变形机制及其与晶粒尺寸的相关性。典型的屈服下降机制,如由于间隙杂质的存在而引起的Cottrell气氛的位错锁定,不能解释UFG高mn奥氏体TWIP钢中这种现象的起源。在此,我们通过实验揭示了变形早期,在宏观屈服点附近的塑性变形机制与晶粒尺寸有明显的关联。更具体地说,随着晶粒尺寸减小到小于1 μm,主要机制由传统的晶粒内部滑移转变为晶界成核孪晶。我们的观察表明,晶粒尺寸依赖的变形机制转变也与不连续屈服行为密切相关,因为它可以控制宏观屈服点周围移动位错的晶粒内部位错密度的变化。
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