S. N. Malik, H. Ahmed, M. Shahid, N. Haider, M. Malik, P. O’Brien
{"title":"Colloidal preparation of copper selenide and indium selenide nanoparticles by single source precursors approach","authors":"S. N. Malik, H. Ahmed, M. Shahid, N. Haider, M. Malik, P. O’Brien","doi":"10.1109/IBCAST.2013.6512127","DOIUrl":null,"url":null,"abstract":"M<sub>x</sub>(<sup>i</sup>Pr<sub>2</sub>PSe<sub>2</sub>)<sub>y</sub>] complexes (M = In, Cu) were synthesized by metathesis reaction of metal with ligand salt [HNEt<sub>3</sub>][<sup>i</sup>Pr<sub>2</sub>PSe<sub>2</sub>]. These complexes undergo thermolysis in HDA/TOP at 200-270 °C, to yield monophasic Cu<sub>2-x</sub>Se and In<sub>2</sub>Se<sub>3</sub> nanoparticles. Cu<sub>2-x</sub>Se nanoparticles (grown at 250 °C) and In<sub>2</sub>Se<sub>3</sub> nanoparticles (grown at 270 °C) had a mean diameter of 5.0 ± 1.2 nm and 13 ± 2.5 nm, respectively.","PeriodicalId":276834,"journal":{"name":"Proceedings of 2013 10th International Bhurban Conference on Applied Sciences & Technology (IBCAST)","volume":"55 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2013-05-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Proceedings of 2013 10th International Bhurban Conference on Applied Sciences & Technology (IBCAST)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/IBCAST.2013.6512127","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3
Abstract
Mx(iPr2PSe2)y] complexes (M = In, Cu) were synthesized by metathesis reaction of metal with ligand salt [HNEt3][iPr2PSe2]. These complexes undergo thermolysis in HDA/TOP at 200-270 °C, to yield monophasic Cu2-xSe and In2Se3 nanoparticles. Cu2-xSe nanoparticles (grown at 250 °C) and In2Se3 nanoparticles (grown at 270 °C) had a mean diameter of 5.0 ± 1.2 nm and 13 ± 2.5 nm, respectively.
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