Stresses evolution at high temperature (200°C) in Copper/Alumina (Cu/Al2O3) stack

N. Doumit, B. Danoumbé, S. Capraro, J. Chatelon, M. Blanc-Mignon, G. Kermouche, J. Rousseau
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Abstract

This paper presents the temperature influence on the adhesion of a copper thin film deposited on an alumina substrate. 5μm and 20 μm thicknesses of copper films were deposited by RF sputtering and characterized. Simulation and mechanical characterizations were realized. Results obtained by Stoney stresses and by Von Mises Stress show stresses relaxation after first annealing and their stabilization for following annealing cycles (200°C). Stress values obtained are lower than the elastic stress on the copper layer which corroborate SEM analysis where copper films present absence of cracks after an annealing at 200°C during one hour. On the other hand, an experimental critical stress characterization has been performed. Results show that critical stress increase with the increasing temperature and decreasing with the copper thickness.
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铜/氧化铝(Cu/Al2O3)叠层高温(200℃)应力演化
本文研究了温度对沉积在氧化铝基体上的铜薄膜附着力的影响。采用射频溅射法制备了厚度为5μm和20 μm的铜膜,并对其进行了表征。实现了仿真和力学表征。通过Stoney应力和Von Mises应力得到的结果表明,在第一次退火后应力松弛,在随后的退火循环(200°C)中应力稳定。得到的应力值低于铜层上的弹性应力,这证实了扫描电镜分析,铜膜在200℃退火1小时后没有出现裂纹。另一方面,进行了实验临界应力表征。结果表明:临界应力随温度的升高而增大,随铜厚度的增加而减小;
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