Synthesis of NiO/ZnO Nanoparticles: Application for Photodegradation of Methylene Blue

Bakhtawar Sajjad, Shaista Ali, Muhammad Akhyar Farrukh
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引用次数: 2

Abstract

NiO/ZnO nanocomposites synthesized by sol-gel method with zinc chloride and nickel nitrate hexahydrate in ethanol used as solvent. Material was characterized by Particle size analyzer, UV-Vis, FTIR, TGA and DSC. NiO/ZnO nanoparticles investigated as a suitable photocatalytic material for the methylene blue degradation i.e. an organic dye under visible light irradiation. The UV–vis absorption spectra of the NiO/ZnO nanoparticles shown peaks in the UV region, corresponding to the band gap of the NiO/ZnO nanoparticles. The band gap of NiO/ZnO nanoparticles is calculated 3.55 eV by Tauc’s plot method. Then UV visible data showed the methylene blue degradation with NiO/ZnO nanoparticles, behaving as active catalyst.
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纳米NiO/ZnO的合成及其在亚甲基蓝光降解中的应用
以六水硝酸镍和氯化锌为溶剂,以乙醇为溶剂,采用溶胶-凝胶法制备了NiO/ZnO纳米复合材料。采用粒度分析仪、紫外-可见光谱、红外光谱、热重分析和差热分析对材料进行了表征。研究了NiO/ZnO纳米颗粒作为可见光下降解亚甲基蓝的合适光催化材料,即有机染料。纳米NiO/ZnO的紫外可见吸收光谱在紫外区出现峰,与纳米NiO/ZnO的带隙相对应。采用Tauc图法计算得到NiO/ZnO纳米粒子的带隙为3.55 eV。紫外可见数据表明,纳米NiO/ZnO对亚甲基蓝的降解具有活性催化剂的作用。
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