Study on carbon fiber surface treatment based on surface oxidation method

Jipeng Zhang, Huicong Tang, Shanshan Hao
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引用次数: 1

Abstract

Surface conditions of carbon fibers severely effect on the bonding strength between the fibers and the matrix, even on the mechanical properties of the composites when carbon fibers were used as reinforcement on the preparation of ceramic matrix composites. Surface treatment of carbon fibers was carried out based on the air oxidation method and the liquid oxidation method with concentrated nitric acid (68%) as the oxidizing solution. It could remove impurities from the surface of carbon fibers and increase the degree of the surface concavoconvex, so the active surface area were increased and then improved the bonding strength between fibers and matrix. The surface topographies of carbon fibers after surface oxidation were characterized by SEM. The results illustrate that, impurities on the surface of carbon fibers are decreased and there are many longitudinal grooves evenly distributed on the surface in favor of increasing the bonding strength between the fibers and matrix.
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基于表面氧化法的碳纤维表面处理研究
碳纤维作为增强材料制备陶瓷基复合材料时,碳纤维的表面状况严重影响纤维与基体的结合强度,甚至影响复合材料的力学性能。以浓硝酸(68%)为氧化溶液,采用空气氧化法和液体氧化法对碳纤维进行表面处理。它可以去除碳纤维表面的杂质,增加表面凹凸度,从而增加活性表面积,从而提高纤维与基体的结合强度。用扫描电镜对碳纤维表面氧化后的形貌进行了表征。结果表明:碳纤维表面杂质减少,表面有许多纵向沟槽均匀分布,有利于提高纤维与基体的结合强度;
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