Annealing and investigation of copper oxide synthesized using coaxial magnetoplasma accelerator

Y. Shanenkova, A. Sivkov, I. Shanenkov, A. Ivashutenko, D. Nikitin
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引用次数: 1

Abstract

The synthesis of copper oxides has a great importance due to the fact these materials are widely used in high temperature superconductors manufacturing. It's known that properties of materials in nanodispersed conditions are improved. In this article, an analysis of nanodispersed plasma dynamic synthesis product obtained using coaxial magnetoplasma accelerator with copper electrodes was carried out. The obtained powder was analyzed by X-ray diffractometer Shimadzu XRD 7000 using the temperature consoles. Using this analysis such phases as Cu, Cu2O, CuO, Cu(OH)2·H2O were identified in the product. By gradually heating, the powder to the temperature of 800 °C the phase change was observed. The mass of copper oxide increased up to 96% and copper hydroxide hydrate.
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同轴磁等离子体加速器合成氧化铜的退火及研究
铜氧化物在高温超导体制造中有着广泛的应用,因此其合成具有重要的意义。在纳米分散的条件下,材料的性能得到了改善。本文对铜电极同轴磁等离子体加速器制备的纳米分散等离子体动态合成产物进行了分析。用x射线衍射仪(Shimadzu XRD 7000)和温度控制仪对所得粉末进行分析。通过分析,确定了产物中Cu、Cu2O、CuO、Cu(OH)2·H2O等相。通过逐渐加热,将粉末加热至800℃,观察其相变。氧化铜和水合氢氧化铜的质量提高到96%。
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