Perovskite-Type Lanthanum Cobaltite LaCoO3: Aspects of Processing Route toward Practical Applications

M. Dragan, S. Enache, M. Varlam, K. Petrov
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引用次数: 8

Abstract

Lanthanum cobaltite (LaCoO3) perovskite-type oxide is an important conductive ceramic material finding a broad range of technical applications. Physical and chemical properties of the final lanthanum cobalt oxide powder material obtained are strongly dependent on the method of preparation. Taking in account these considerations, we focus our investigation on the solid state reaction process. The characterization of prepared lanthanum cobalt oxide material was studied by using X-ray diffractometry (XRD), scanning electron microscopy (SEM), thermogravimetry-differential scanning calorimetry (TG-DSC), and conduction properties. Following the experimental results, it can be concluded that with proper improvement, the solid state reaction process may also provide an efficient preparation method for perovskite-type LaCoO3 powder. Important to mention is that we looked into the aspects to produce again same which showed consistently reproducibility of batch to batch powder properties. This is a key factor to overcome a successful commercialization of new material synthesis development.
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钙钛矿型钴酸镧LaCoO3:走向实际应用的加工路线
钴酸镧(LaCoO3)钙钛矿型氧化物是一种重要的导电陶瓷材料,具有广泛的技术应用。最终得到的氧化镧粉末材料的物理和化学性质在很大程度上取决于制备方法。考虑到这些因素,我们将研究重点放在固态反应过程上。采用x射线衍射(XRD)、扫描电镜(SEM)、热重-差示扫描量热法(TG-DSC)和导电性能对制备的氧化钴镧材料进行表征。根据实验结果,可以得出结论,通过适当的改进,固相反应工艺也可以为钙钛矿型LaCoO3粉末的制备提供一种有效的方法。重要的是要提到的是,我们研究了生产相同的方面,这表明了批到批粉末性能的一致性再现性。这是克服新材料合成开发成功商业化的关键因素。
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