Processing and Functional Evaluation of Titanium Thin Films for Biomimetic Micro Actuator

T. Sakai, Sodai Hoshiai, E. Nakamachi
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引用次数: 1

Abstract

Titanium (Ti) thin films were created on glass and Pb(Zr, Ti)O3 (PZT) substrates using magnetic RF sputtering apparatus. Nano-indentation tests were carried out to study the influence of the Ti thin layer on piezoelectric properties. The piezoelectric properties of the PZT plate and a Ti sputtered one were also measured by laser Doppler vibrometer. Furthermore, some characteristics, such as crystalline structure, depth profiles, and surface roughness of the films were observed by means of an atomic force microscope (AFM). Main conclusions obtained in this study are summarized as follows: (1) From detailed observation and analytical results of AFM, the surface roughness, Ra, tends to increase as Ti film thickness increases. (2) Some of the mechanical properties, such as reduced modulus Er and hardness H obtained from nano-indentation tests, are significantly related to film thickness. (3) The validity of piezoelectric finite element analysis (ANASYS program) for deformation of a piezoelectric material was investigated. As a result, piezoelectric response properties are present in as-received PZT specimens and Ti-sputtered PZT specimens. Experimental and FE analytical results indicate that the piezoelectric coefficient is significantly influenced by Ti layer.
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仿生微驱动器用钛薄膜的制备及功能评价
采用射频磁溅射装置在玻璃和Pb(Zr, Ti)O3 (PZT)衬底上制备了钛(Ti)薄膜。采用纳米压痕试验研究了Ti薄层对压电性能的影响。用激光多普勒振动仪测量了PZT板和Ti溅射板的压电性能。此外,利用原子力显微镜(AFM)观察了薄膜的晶体结构、深度分布和表面粗糙度等特征。本研究的主要结论总结如下:(1)从AFM的详细观察和分析结果来看,表面粗糙度Ra随Ti膜厚度的增加而增加。(2)纳米压痕试验获得的一些力学性能,如降低模量Er和硬度H,与薄膜厚度显著相关。(3)研究了压电有限元分析(ansys程序)对压电材料变形的有效性。结果表明,接收态PZT试样和ti溅射态PZT试样均具有压电响应特性。实验和有限元分析结果表明,Ti层对压电系数有显著影响。
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