AE Monitoring of Microdamages in Bioceramics for Artificial Joints under Simulated Body Environment

S. Wakayama, Yasuhiro Suzuki, T. Oshima, Satoshi Kobayashi
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引用次数: 1

Abstract

Microfracture process of 3 mol% yttria stabilized zirconia (3Y-TZP) for artificial joints was evaluated using the acoustic emission technique. In order to investigate the e ff ects of environment and strain rate on the microfracture process, four point bending tests were carried out in air and physiological saline (P.S.) at various loading rates. From the results of AE behavior, rapid AE increasing point was observed before the final unstable fracture. It was suggested from the previous work that the AE increasing point corresponds to the maincrack formation. The critical stress for maincrack formation, σ C , was determined from the bending stress at the AE increasing point. The critical stress as well as bending strength, σ B , decreased in physiological saline. In particular, the decrease in critical stress was remarkable. It was then understood that stress corrosion cracking (SCC) by water in physiological saline a ff ected maincrack formation rather than the final fracture. Consequently, it was suggested that the evaluation of σ C is essential for the reliability assessment of bioceramics.
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模拟人体环境下生物陶瓷人工关节微损伤的声发射监测
采用声发射技术对3mol %氧化钇稳定氧化锆(3Y-TZP)用于人工关节的微断裂过程进行了评价。为了研究环境和应变速率对微断裂过程的影响,在空气和生理盐水中进行了不同加载速率下的四点弯曲试验。从声发射行为的结果来看,在最终的不稳定断裂之前,出现了快速的声发射增加点。前人的研究表明,声发射的增加点与主裂纹的形成相对应。主裂纹形成的临界应力σ C由声发射增量处的弯曲应力确定。在生理盐水中,临界应力和抗弯强度σ B均有所降低。特别是,临界应力的降低是显著的。后来人们认识到,生理盐水中的应力腐蚀开裂(SCC)影响的是主裂缝的形成,而不是最终裂缝。因此,σ C的评价是生物陶瓷可靠性评价的必要条件。
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