Enhancing the light fastness of tannin from mangrove waste by encapsulation with chitosan nanoparticle

Totok Hendarto, Didik Budiyanto
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Abstract

Microwave assisted extraction is an environmentally friendly extraction method, which has been used to extract tannins from mangrove waste. Tannin is a natural dye which is easily oxidized, easily degraded and the color fades easily. To increase its color retention, tannin was encapsulated with chitosan nanoparticle. This study aims to determine the effect of volume tween 80 on particle size and physical and chemical characteristics of tannin extract from mangroves encapsulated with chitosan nanoparticle. The encapsulated tannin extract particle size was measured by Particle Size Analyzer and characterized by FTIR, SEM. The test results showed that the average particle diameter of the encapsulated tannin extract was in the range of 192.37 nm with a PDI of 0.1660 which was obtained by adding 0.5 mL of Tween 80. Encapsulation efficiency reaches 78.1%. The FTIR spectrum showed the presence of a cross-linked C=N stretching absorption band at wave number 1643.35 cm-1 in nano encapsulation of tannin extract.. The color fastness test of cotton cloth in hot water has a value of ΔE = 3, which means that the color fastness is moderate.
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壳聚糖纳米粒包封提高红树林废弃物单宁的耐光性
微波辅助提取是一种环保的提取方法,已被用于从红树林废弃物中提取单宁。单宁是一种易氧化、易降解、易褪色的天然染料。为了提高单宁的保色性,用壳聚糖纳米颗粒包封单宁。本研究旨在研究壳聚糖纳米颗粒包封后,体积吐温80对红树林单宁提取物粒径及理化性质的影响。采用粒度分析仪测定了包封后的栲胶的粒径,并用FTIR、SEM对其进行了表征。实验结果表明,当添加0.5 mL吐温80时,包封的单宁提取物的平均粒径为192.37 nm, PDI为0.1660。封装效率达78.1%。红外光谱分析表明,单宁提取物在1643.35 cm-1波长处存在一个交联的C=N拉伸吸收带。棉布在热水中的色牢度试验值ΔE = 3,表示色牢度适中。
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