Direct Correlation of the Crack Distribution in APS Thermal Barrier Coatings with the Measured Synchrotron XRD Residual Stress Distribution

C. Lia, R. Cernik
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Abstract

Residual stress distributions as a function of depth in APS TBCs after different heat treatment times have been measured by synchrotron XRD. Three types of residual stress distribution were observed. The first type was a low stress state from the as-received sample; the second type was a compressive stress state increasing from the surface to the interface with a discontinuous "jump feature" in the trend near the interface; the third type of residual stress distribution has two "jump" features in the trend, one was observed near the sample surface and the other near the interface. To understand the double "jump" features in the third kind of trend, the 3D microstructures of the measured samples were systematically measured X-ray μ-CT. Vertical cracks and edge cracks were observed. We have shown by image based modelling that the vertical cracks do not have a large effect on the residual stress distribution and that edge cracks are related to the "jump features" near the sample surface. The edge crack can be observed in all the measured samples with the third kind of the residual stress trend; and the measured samples with the second kind of the residual stress trend are crack free. The relationship between the middle and the through edge cracks and the residual stress distribution was also investigated by image based modelling. It was found that the middle crack can also cause a "jump feature" near the sample surface while the through edge crack seems to not have a large effect on the residual stress distribution. A semi-destructive method was developed to determine the existence and the position of horizontal cracks in the APS TBC samples based on the above findings.
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APS热障涂层裂纹分布与同步加速器x射线衍射残余应力分布的直接关系
采用同步加速器x射线衍射仪(XRD)测量了不同热处理次数后APS tbc中残余应力随深度的分布。观察到三种类型的残余应力分布。第一种是接收样品的低应力状态;第二种是压应力从表面向界面递增,在界面附近呈不连续的“跳变”趋势;第三类残余应力分布在趋势上有两个“跳跃”特征,一个在试样表面附近,另一个在界面附近。为了解第三种趋势的双“跳变”特征,采用x射线μ-CT系统测量了被测样品的三维显微结构。观察到垂直裂纹和边缘裂纹。我们已经通过基于图像的建模表明,垂直裂缝对残余应力分布没有很大的影响,边缘裂缝与样品表面附近的“跳跃特征”有关。所有试样均存在边缘裂纹,残余应力趋势均为第三种;第二种残余应力趋势下的试样无裂纹。采用基于图像的建模方法研究了中间裂纹和贯通裂纹与残余应力分布的关系。发现中间裂纹也会引起试样表面附近的“跳跃特征”,而贯通边缘裂纹对残余应力分布的影响似乎不大。在此基础上,提出了一种半破坏性的方法来确定APS TBC试样中水平裂纹的存在和位置。
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