Synthesis of silver nanoparticles with polyols under reflux and microwave irradiation conditions

IF 0.5 4区 化学 Q4 CHEMISTRY, MULTIDISCIPLINARY Chemija Pub Date : 2023-09-17 DOI:10.6001/chemija.2023.34.3.1
Edita Daublytė, Marija Kalnaitytė, Aliona Klimovich, Audrius Drabavičius, Tatjana Charkova
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Abstract

Four polyols were used as stabilisers to synthesise silver nanospheres under reflux and microwave irradiation conditions. The nanoparticles were covered with a protective up to 10 nm silicon dioxide shell. The shell-isolated nanoparticle-enhanced Raman spectroscopy (SHINERS) technique was used to analyse the self-assembled monolayer of 4-mercaptobenzoic acid (4-MBA) by applying the produced silver core-silica shell nanoparticles. The article provides a detailed description of the synthesis, analysis and application of the nanoparticles based on UV/Vis, HR-TEM and SHINERS data.
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多元醇在回流和微波辐照条件下合成纳米银
以四种多元醇为稳定剂,在回流和微波辐照条件下合成纳米银球。纳米颗粒被一层长达10纳米的二氧化硅保护壳覆盖。利用壳隔离纳米粒子增强拉曼光谱(SHINERS)技术,利用制备的银核-硅壳纳米粒子对4-巯基苯甲酸(4-MBA)自组装单层进行了分析。本文基于UV/Vis、HR-TEM和SHINERS数据详细介绍了纳米颗粒的合成、分析和应用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Chemija
Chemija 化学-化学综合
CiteScore
1.30
自引率
16.70%
发文量
14
审稿时长
>12 weeks
期刊介绍: Chemija publishes original research articles and reviews from all branches of modern chemistry, including physical, inorganic, analytical, organic, polymer chemistry, electrochemistry, and multidisciplinary approaches.
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