Three-Dimensional Analysis of Porosity in As-Manufactured Glass Fiber/Vinyl Ester Filament Winded Composites Using X-Ray Micro-Computed Tomography

IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Applied Composite Materials Pub Date : 2023-10-19 DOI:10.1007/s10443-023-10167-z
Chaman Srivastava, Pietro Agostino, Antonios G. Stamopoulos, Ben Alcock, Are Strandlie, Sotirios Grammatikos
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Abstract

Filament winding is a technique to manufacture tubular composite structures and, therefore, is among the most appealing techniques for fabricating critical structures such as hollow tubes. Despite the recent advances, these structures are prone to a varying degree of porosity that may affect their mechanical performance. Therefore, the accurate detection and quantification of the manufacturing porosity is crucial. Micro-CT is most suitable for performing this activity at various scales. This work employs micro-CT for studying porosity inside an as-manufactured filament-winded composite structure. Void characteristics like volume, orientation, size, and relative volume fraction inside the hoop and helical layers are quantified inside a representative curved panel extracted from a glass fiber-vinyl ester tubular composite structure, which has not been studied in detail previously. It was observed that most voids are present in the matrix region. The voids are elliptical rod-like and spherical, with the latter present in the helical layers, which also host the majority of voids and the highest void volume fractions. The voids are highly aligned along the fiber orientation direction with higher misorientations for helical layers than the hoop layer. Large voids in base layers were created due to gaps formed during the winding process. Hence, the main goal of this study is to measure the voids' characteristics and the volumetric fraction during the stacking of filament wound hoop and helical layers during a generic filament winding pattern. The data can be further exploited as input for modeling filament winded composites in the presence of voids by researchers.

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利用 X 射线显微计算机断层扫描技术三维分析玻璃纤维/乙烯基酯长丝缠绕复合材料成品中的孔隙率
纤丝缠绕是一种制造管状复合材料结构的技术,因此是制造空心管等关键结构的最有吸引力的技术之一。尽管最近取得了一些进步,但这些结构仍容易出现不同程度的孔隙,从而影响其机械性能。因此,准确检测和量化制造孔隙率至关重要。微计算机断层扫描最适合在各种尺度上开展这项工作。本研究采用显微计算机断层扫描技术来研究制造完成的丝卷复合材料结构内部的孔隙率。从玻璃纤维-乙烯基酯管状复合材料结构中提取的具有代表性的弧形面板内的空隙特征,如箍层和螺旋层内的空隙体积、取向、大小和相对体积分数都进行了量化。结果表明,大部分空隙存在于基体区域。空隙分为椭圆杆状和球状,后者存在于螺旋层中,也是空隙最多、空隙体积分数最高的地方。空隙沿纤维取向方向高度排列,螺旋层的取向错误率高于环形层。由于缠绕过程中形成的间隙,基底层中产生了大量空隙。因此,本研究的主要目标是测量长丝缠绕环形层和螺旋层在一般长丝缠绕模式下堆叠过程中的空隙特征和体积分数。研究人员可进一步利用这些数据,为存在空隙的长丝缠绕复合材料建模。
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来源期刊
Applied Composite Materials
Applied Composite Materials 工程技术-材料科学:复合
CiteScore
4.20
自引率
4.30%
发文量
81
审稿时长
1.6 months
期刊介绍: Applied Composite Materials is an international journal dedicated to the publication of original full-length papers, review articles and short communications of the highest quality that advance the development and application of engineering composite materials. Its articles identify problems that limit the performance and reliability of the composite material and composite part; and propose solutions that lead to innovation in design and the successful exploitation and commercialization of composite materials across the widest spectrum of engineering uses. The main focus is on the quantitative descriptions of material systems and processing routes. Coverage includes management of time-dependent changes in microscopic and macroscopic structure and its exploitation from the material''s conception through to its eventual obsolescence.
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