Study of the Structural Properties of NiCl2:Al2O3 Thin Film Prepared by Chemical Thermal Spraying Technique

Mohamed Khaled Khalil Yasin, Raheem G. Kadhim Hussein, Saba Abdul Zahra Obaid Alshiaa
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Abstract

Background: The structural properties of films are studied by several techniques, and X-ray diffraction (XRD) is one of the most reliable methods that were adopted in this research, so will explain it in some detail, in addition to assays (SEM ) that give information on surface morphology. Materials and Methods: The thermochemical spraying technique was used to prepare the thin films. Results: The results showed that increasing the temperature led to a decrease in the average particle size, in contrast to the doping process. Conclusion: The reason for the decrease in particle size is due to the increase in the Full Width at Half Maximum (FWHM) in addition to an increase in the crystallization of the thin films, and also the membrane becomes more regular and crystalline defects decrease and increase.
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化学热喷涂法制备NiCl2:Al2O3薄膜的结构性能研究
背景:薄膜的结构特性是通过几种技术来研究的,x射线衍射(XRD)是本研究中采用的最可靠的方法之一,所以除了分析(SEM)提供表面形貌信息外,我们还将详细解释它。材料与方法:采用热化学喷涂技术制备薄膜。结果:与掺杂工艺相反,温度升高导致平均粒径减小。结论:颗粒尺寸减小的原因是由于薄膜的半最大全宽(FWHM)增加,薄膜的结晶性增加,膜变得更加规则,晶体缺陷减少和增加。
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