Characterization of Interlaminar Static and Fatigue Delamination Growth in Carbon/Epoxy Composites Reinforced with Carbon Nanotubes

IF 2.3 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Applied Composite Materials Pub Date : 2023-11-16 DOI:10.1007/s10443-023-10170-4
Millan Kumar, Pramod Kumar, Shailendra Singh Bhadauria
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Abstract

The present study focuses on the effect of CNT nanofillers on the interlaminar static and fatigue crack propagation in carbon fiber reinforced composite laminates. Multi-walled carbon nanotubes (MWCNTs) were dispersed over the laminate interface through solvent spraying technique. The mode I fracture toughness and R curve behavior were determined first from DCB specimens. Then, the fatigue tests were performed at different stress ratios for laminates containing different contents of CNTs to determine the delamination growth rate da/dN from fatigue crack growth (FCG) curves. When FCG curves are expressed as a function of G, where G is the energy release rate, the growth curves are dependent on the R-ratio. It was found that the addition of CNTs enhances the delamination resistance in the initial part of FCG curves, i.e. low cyclic region. As the test progresses, the effect gradually diminishes making nanofillers ineffective. It is then shown that the FCG curves can be characterized when crack growth rates are expressed as a function of the crack‐driving force \(\overline{\Delta \kappa }\) used in the Hartman‐Schijve equation. Therefore, the present paper presents a methodology to account for the stress ratio effect to evaluate the crack growth rate for any given R-ratio and to obtain a valid, upper-bound FCG rate curves in CNT reinforced laminates that exhibit high degree of scatter.

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碳纳米管增强碳/环氧复合材料层间静态和疲劳脱层生长的表征
本文主要研究了碳纳米管填充剂对碳纤维增强复合材料层间静力和疲劳裂纹扩展的影响。采用溶剂喷涂技术将多壁碳纳米管(MWCNTs)分散在层压板界面上。首先从DCB试样中测定了I型断裂韧性和R曲线行为。然后,对含不同碳纳米管含量的层合材料进行不同应力比下的疲劳试验,从疲劳裂纹扩展(FCG)曲线中确定分层扩展速率da/dN。当FCG曲线表示为G的函数时,其中G为能量释放率,生长曲线依赖于r比。研究发现,CNTs的加入增强了FCG曲线初始部分,即低循环区域的抗分层能力。随着试验的进行,效果逐渐减弱,纳米填料失效。然后表明,当裂纹扩展速率表示为Hartman - Schijve方程中裂纹驱动力\(\overline{\Delta \kappa }\)的函数时,可以表征FCG曲线。因此,本文提出了一种考虑应力比效应的方法,以评估任何给定r比下的裂纹扩展速率,并获得碳纳米管增强层合板中具有高度分散的有效的上限FCG速率曲线。
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来源期刊
Applied Composite Materials
Applied Composite Materials 工程技术-材料科学:复合
CiteScore
4.20
自引率
4.30%
发文量
81
审稿时长
1.6 months
期刊介绍: Applied Composite Materials is an international journal dedicated to the publication of original full-length papers, review articles and short communications of the highest quality that advance the development and application of engineering composite materials. Its articles identify problems that limit the performance and reliability of the composite material and composite part; and propose solutions that lead to innovation in design and the successful exploitation and commercialization of composite materials across the widest spectrum of engineering uses. The main focus is on the quantitative descriptions of material systems and processing routes. Coverage includes management of time-dependent changes in microscopic and macroscopic structure and its exploitation from the material''s conception through to its eventual obsolescence.
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