Pycnometric-Additive Determining of the Degree of Coating of High-Strength Synthetic Diamond Grinding Powders using the Actual 3D Morphology of their Grains

G. A. Petasyuk, O. O. Bochechka, V.I. Lavrinenko, V. Poltoratskyi, Yulia Syrota, V. P. Bilochenko
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Abstract

The methodological components of direct and indirect analytical determining of the degree of coating of synthetic diamond grinding powders are analyzed. It has been established that the weight method most used in practice for determining this technological property of grinding powder is not universal for different methods of applying the coating. More universal in this regard, as the review of publications showed, is the well-known indirect-analytical method based on the pycnometric-additive approach. An improved variant of this method is proposed, aimed at application to high-strength synthetic diamond grinding powders. The method takes into account the peculiarities of the 3D morphology of the grains of such powders. Using the example of grinding powder AC300 500/400, the grains of which were coated with a solution of a mixture of boron oxide, sodium silicate, and titanium carbide, the advantages of using the proposed method are illustrated. The results of a comparison of determining the degree of coating by a known method and its improved variant are presented.
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利用高强度人造金刚石磨粉晶粒的实际 3D 形态以 Pycnometric 附加法测定其涂层度
对直接和间接分析确定人造金刚石磨粉涂层程度的方法进行了分析。结果表明,在实践中最常用于测定研磨粉技术特性的重量法并不适用于不同的涂层方法。正如文献综述所显示的那样,在这方面更通用的是著名的间接分析方法,该方法基于比重加成法。本文提出了该方法的改进版,旨在应用于高强度合成金刚石磨粉。该方法考虑到了此类粉末颗粒三维形态的特殊性。以研磨粉 AC300 500/400 为例,说明了使用该方法的优势,该研磨粉的颗粒上涂有氧化硼、硅酸钠和碳化钛的混合物溶液。此外,还介绍了通过已知方法和改进变体确定涂层程度的比较结果。
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