Characterization of nano-hydroxyapatite synthesized from eggshells for absorption of heavy metals

Leila Karamzadeh, E. Salahi, I. Mobasherpour, Armin Rajabi, Masomeh Javaheri
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Abstract

This paper presents the synthesis of nano hydroxyapatite using deposition process and eggshell as a cost-effective starting material. This study investigates its potential as an effective adsorbent for heavy metals. Various analytical techniques, including X-ray diffraction (XRD), X-ray fluorescence spectroscopy (XRF), Fourier transform infrared (FTIR), surface area measurement (BET), and scanning electron microscopy (SEM), were used to characterize the composition. The main objective was to evaluate the suitability of the synthesized hydroxyapatite as a heavy metal adsorbent in aqueous solutions. The results of this research showed that hydroxyapatite, which has a particle size in the range of nanometers and a specific area of 150 square meters per gram, and has the necessary properties for absorption, was successfully processed. The results showed that the prepared samples had a uniform mesopore distribution between 2 and 3 nm and 6 and 20 nm.
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利用蛋壳合成的纳米羟基磷灰石在吸收重金属方面的表征
本文介绍了利用沉积工艺和蛋壳作为成本效益高的起始材料合成纳米羟基磷灰石的方法。本研究探讨了其作为重金属有效吸附剂的潜力。研究采用了多种分析技术,包括 X 射线衍射 (XRD)、X 射线荧光光谱 (XRF)、傅立叶变换红外 (FTIR)、表面积测量 (BET) 和扫描电子显微镜 (SEM) 来表征其成分。主要目的是评估合成的羟基磷灰石作为水溶液中重金属吸附剂的适用性。研究结果表明,羟基磷灰石的粒度在纳米范围内,每克的比面积为 150 平方米,具有吸附所需的特性。结果表明,制备的样品在 2 至 3 纳米和 6 至 20 纳米之间具有均匀的中孔分布。
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