Effects of die geometry and insulation on the energy and electrical parameters analyses of spark plasma sintered TiC ceramics

Milad Sakkaki, Milad Foroutani, Peyman Zare
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Abstract

This work conducts a numerical simulation to investigate the temperature and electric current distribution during the spark plasma sintering (SPS) process using the finite element method (FEM) carried out in COMSOL Multiphysics software. The main goal is to optimize the SPS process for titanium carbide (TiC) ceramics, with a particular focus on the effects of insulation and die geometry (height and thickness). For the TiC material, the ideal sintering temperature is set at 2000 °C. The study analyzes eight case studies, involving a base case, an insulating case, and six cases with various thicknesses and heights, in order to evaluate the effectiveness of the suggested optimization. The results show that using insulation on the die surface reduces heat transfer from the die surface significantly, which leads to a 63% decrease in input power consumption when compared to the basic scenario. Based on a correlation study between energy and electricity, increasing die thickness raises the cross-sectional area of the electric current, which raises the amount of electric power required to attain the 2000 °C sintering temperature. The results indicate the temperature distribution in the sample is more sensitive to changes in die height than to changes in die thickness.
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模具几何形状和绝缘对火花等离子烧结 TiC 陶瓷的能量和电气参数分析的影响
本研究使用 COMSOL Multiphysics 软件中的有限元法 (FEM) 进行数值模拟,研究火花等离子烧结 (SPS) 过程中的温度和电流分布。主要目标是优化碳化钛(TiC)陶瓷的 SPS 工艺,尤其关注绝缘和模具几何形状(高度和厚度)的影响。对于 TiC 材料,理想的烧结温度设定为 2000 ℃。研究分析了八个案例,包括一个基本案例、一个绝缘案例和六个具有不同厚度和高度的案例,以评估建议优化的有效性。结果表明,在芯片表面使用隔热材料可显著减少芯片表面的热传递,与基本方案相比,输入功耗降低了 63%。根据能量和电力之间的相关性研究,增加模具厚度会增加电流的横截面积,从而增加达到 2000 °C 烧结温度所需的电力。结果表明,样品中的温度分布对模具高度的变化比模具厚度的变化更为敏感。
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