Interfacial microstructure and mechanical properties of Si3N4/Invar joints using Ag–Cu–In–Ti with Cu foil as an interlayer

IF 2.4 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Testing Pub Date : 2024-01-11 DOI:10.1515/mt-2023-0221
Tong Zhao, Defeng Mo, Xue Li, Haimei Gong
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Abstract

Abstract Si3N4 and Invar alloy brazed joints were achieved using two types of Ag-based interlayers: a Ag–Cu–In–Ti foil and a Ag–Cu–In–Ti/Cu/Ag–Cu multi-interlayer. The results showed that when only using a single Ag–Cu–In–Ti filler, the wave-shaped Fe2Ti + Ni3Ti intermetallic compounds are concentrated in the middle of the brazing seam. When adding Cu as the interlayer, the dissolution of the Cu interlayer formed a large number of Cu(s,s) blocks of different sizes in the brazing seam, which hindered the concentrated distribution of Fe2Ti + Ni3Ti intermetallic compounds in the brazing seam. As a result, Fe2Ti and Ni3Ti were dispersedly distributed in the brazing seam, increasing the shear strength of the brazed joint. The shear strength of brazed joints was increased by 82 % compared to joints brazed with a single Ag–Cu–In–Ti filler when the Cu interlayer was added.
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以铜箔为中间层的银铜铟锡 Si3N4/Invar 接头的界面微观结构和力学性能
摘要 使用两种类型的银基中间膜实现了 Si3N4 和英华合金钎焊接缝:一种是银-铜-铟-钛箔,另一种是银-铜-铟-钛/铜/银-铜多层中间膜。结果表明,只使用单一的银-铜-铟-钛填料时,波浪形的 Fe2Ti + Ni3Ti 金属间化合物集中在钎缝的中间。当加入 Cu 作为中间层时,Cu 中间层的溶解在钎缝中形成了大量大小不一的 Cu(s,s)块,阻碍了 Fe2Ti + Ni3Ti 金属间化合物在钎缝中的集中分布。因此,Fe2Ti 和 Ni3Ti 在钎缝中分散分布,提高了钎焊接头的抗剪强度。当加入铜中间层时,钎焊接头的剪切强度比使用单一银-铜-铟-钛填料钎焊的接头提高了 82%。
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来源期刊
Materials Testing
Materials Testing 工程技术-材料科学:表征与测试
CiteScore
4.20
自引率
36.00%
发文量
165
审稿时长
4-8 weeks
期刊介绍: Materials Testing is a SCI-listed English language journal dealing with all aspects of material and component testing with a special focus on transfer between laboratory research into industrial application. The journal provides first-hand information on non-destructive, destructive, optical, physical and chemical test procedures. It contains exclusive articles which are peer-reviewed applying respectively high international quality criterions.
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