Isolated scan unit and scanning tunneling microscope for stable imaging in ultra-high magnetic fields

IF 2.1 3区 工程技术 Q2 MICROSCOPY Ultramicroscopy Pub Date : 2024-03-22 DOI:10.1016/j.ultramic.2024.113960
Jihao Wang , Zihao Li , Kesen Zhao , Shuai Dong , Dan Wu , Wenjie Meng , Jing Zhang , Yubin Hou , Yalin Lu , Qingyou Lu
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Abstract

The high resolution of a scanning tunneling microscope (STM) relies on the stability of its scan unit. In this study, we present an isolated scan unit featuring non-magnetic design and ultra-high stability, as well as bidirectional movement capability. Different types of piezoelectric motors can be incorporated into the scan unit to create a highly stable STM. The standalone structure of scan unit ensures a stable atomic imaging process by decreasing noise generated by motor. The non-magnetic design makes the scan unit work stable in high magnetic field conditions. Moreover, we have successfully constructed a novel STM based on the isolated scan unit, in which two inertial piezoelectric motors act as the coarse approach actuators. The exceptional performance of homebuilt STM is proved by the high-resolution atomic images and dI/dV spectrums on NbSe2 surface at varying temperatures, as well as the raw-data images of graphite obtained at ultra-high magnetic fields of 23 T. According to the literature research, no STM has previously reported the atomic image at extreme conditions of 2 K low temperature and 23 T ultra-high magnetic field. Additionally, we present the ultra-low drift rates between the tip and sample at varying temperatures, as well as when raising the magnetic fields from 0 T to 23 T, indicating the ultra-high stability of the STM in high magnetic field conditions. The outstanding performance of our stable STM hold great potential for investigating the materials in ultra-high magnetic fields.

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用于在超高磁场中稳定成像的隔离式扫描单元和扫描隧道显微镜
扫描隧道显微镜(STM)的高分辨率取决于其扫描单元的稳定性。在这项研究中,我们提出了一种具有非磁性设计和超高稳定性以及双向移动能力的隔离式扫描单元。不同类型的压电电机可以集成到扫描单元中,从而制造出高度稳定的 STM。扫描单元的独立结构可降低电机产生的噪音,从而确保原子成像过程的稳定性。非磁性设计使扫描单元在高磁场条件下也能稳定工作。此外,我们还成功地构建了一种基于隔离式扫描单元的新型 STM,其中两个惯性压电电机充当粗准执行器。我们在不同温度下获得了 NbSe2 表面的高分辨率原子图像和 dI/dV 光谱,并在 23 T 超高磁场条件下获得了石墨的原始数据图像,这些都证明了自制 STM 的卓越性能。此外,我们还展示了在不同温度下以及将磁场从 0 T 提高到 23 T 时针尖与样品之间的超低漂移率,这表明 STM 在高磁场条件下具有超高稳定性。我们稳定的 STM 的出色性能为研究超高磁场中的材料提供了巨大的潜力。
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来源期刊
Ultramicroscopy
Ultramicroscopy 工程技术-显微镜技术
CiteScore
4.60
自引率
13.60%
发文量
117
审稿时长
5.3 months
期刊介绍: Ultramicroscopy is an established journal that provides a forum for the publication of original research papers, invited reviews and rapid communications. The scope of Ultramicroscopy is to describe advances in instrumentation, methods and theory related to all modes of microscopical imaging, diffraction and spectroscopy in the life and physical sciences.
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