Separation of milk fat using silicon carbide support ceramic membranes with different pore sizes

IF 6.3 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Innovative Food Science & Emerging Technologies Pub Date : 2024-04-17 DOI:10.1016/j.ifset.2024.103671
Tobias Dons , Victor Candelario , Ulf Andersen , Lilia Ahrné
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Abstract

The effect of pore size and type of material on the separation of fat from raw milk using hydrophilic silicon carbide (SiC) support ceramic membranes has not previously been reported in literature. The separation performance of the fat globules (MFGs) showed 98% for SiC 0.5 μm, 92% for SiC 1.4 μm, 90% fat for ZrO2-SiC 0.06 μm, while the permeate had a fat % ranging from 0.1 to 0.6% (w/w). The MFGs were kept highly intact with well distributed proteins and phospholipids in the MFG membrane. The total filtration time at 50 °C to reach maximum VCR was 134 min for ZrO2 (VCR 3), 148 min for SiC 0.5 μm and 16 min for SiC 1.4 μm (VCR4). Further, all membranes showed a fully recoverable water permeability indicating no irreversible fouling.

Industrial relevance

Microfiltration may be an alternative process to fat separation from raw milk. In this study, for the first time was demonstrated that effective milk fat separation, and retentate and permeate streams with variable characteristics, in terms of composition and integrity of the milk fat globules can be obtained by using silicon carbide support membranes with different sizes and materials. The results obtained, provide new insights for industrial use of membrane technology to separate milk.

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使用不同孔径的碳化硅支撑陶瓷膜分离牛奶脂肪
使用亲水性碳化硅(SiC)支撑陶瓷膜分离原料奶中的脂肪时,孔径大小和材料类型对其分离效果的影响此前尚未见文献报道。碳化硅 0.5 μm 的脂肪球(MFGs)分离率为 98%,碳化硅 1.4 μm 的分离率为 92%,ZrO2-碳化硅 0.06 μm 的脂肪分离率为 90%,而渗透物的脂肪含量为 0.1% 至 0.6%(重量比)。MFG 保持高度完整,蛋白质和磷脂在 MFG 膜上分布均匀。在 50 °C 条件下,达到最大 VCR 的总过滤时间分别为:ZrO2 134 分钟(VCR 3)、SiC 0.5 μm 148 分钟和 SiC 1.4 μm 16 分钟(VCR 4)。此外,所有膜都显示出完全可恢复的透水性,表明没有不可逆的污垢。这项研究首次证明,使用不同尺寸和材料的碳化硅支撑膜可以有效分离牛奶脂肪,并获得在牛奶脂肪球的组成和完整性方面具有不同特性的回流液和渗透液。所获得的结果为工业上使用膜技术分离牛奶提供了新的思路。
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来源期刊
CiteScore
12.00
自引率
6.10%
发文量
259
审稿时长
25 days
期刊介绍: Innovative Food Science and Emerging Technologies (IFSET) aims to provide the highest quality original contributions and few, mainly upon invitation, reviews on and highly innovative developments in food science and emerging food process technologies. The significance of the results either for the science community or for industrial R&D groups must be specified. Papers submitted must be of highest scientific quality and only those advancing current scientific knowledge and understanding or with technical relevance will be considered.
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