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Citrus by-products: A dual assessment of antioxidant properties and food contaminants towards circular economy 柑橘副产品:实现循环经济的抗氧化性和食品污染物双重评估
IF 6.3 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-07-01 DOI: 10.1016/j.ifset.2024.103737
Ana Rita Soares Mateus , Sandra Mariño-Cortegoso , Sílvia Cruz Barros , Raquel Sendón , Letricia Barbosa , Angelina Pena , Ana Sanches-Silva

Orange, lemon, and lime by-products emerge as promising sources of phenolic compounds. This study presents the first comprehensive assessment of the antioxidant capacity and food safety considerations of citrus pomace, aiming for their safe integration into the food industry. Results reveal that lemon and lime by-products are particularly rich in eriocitrin, hesperidin, trans-ferulic acid, and p-coumaric acid, significantly contributing to their antioxidant capacity. Regarding food safety, none of the nine regulated mycotoxins were detected. However, heavy metals were present below the maximum levels. Furthermore, pesticide residues were present, although at low levels in most cases. Contrarily, lime by-product presented high levels of the flutriafol. This study highlights the value of citrus by-products as source of natural antioxidants and emphasizes the necessity of monitoring and mitigating pesticide residues for their safe incorporation into functional food products. These findings support the sustainable utilization of citrus pomace within the circular economy framework, offering opportunities for innovation in the food industry.

柑橘、柠檬和酸橙的副产品是酚类化合物的重要来源。这项研究首次对柑橘渣的抗氧化能力和食品安全因素进行了全面评估,旨在将其安全地融入食品工业。研究结果表明,柠檬和酸橙的副产品中含有特别丰富的麦角苷、橙皮甙、反式阿魏酸和对香豆酸,大大提高了它们的抗氧化能力。在食品安全方面,没有检测到九种受管制的霉菌毒素。不过,重金属含量低于最高水平。此外,还发现了农药残留,不过大多数情况下含量都很低。相反,石灰副产品中的氟三唑含量较高。这项研究突出了柑橘副产品作为天然抗氧化剂来源的价值,并强调了监测和减少农药残留的必要性,以便将其安全地添加到功能性食品中。这些研究结果支持在循环经济框架内可持续地利用柑橘渣,为食品工业的创新提供了机会。
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引用次数: 0
A novel electro-mechanical chewing system for food oral processing research: A comprehensive design approach 用于食品口腔加工研究的新型电动机械咀嚼系统:综合设计方法
IF 6.3 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-07-01 DOI: 10.1016/j.ifset.2024.103735
Sandip Panda , Naama Degany , Xiaofeng Zhang , Jianshe Chen , Avi Meirowitz , Rachel Sarig , Ofir Benjamin

This paper presents a comprehensive design approach for an electro-mechanical system for food oral processing research. The bespoke design and prototype of the proposed device is a standalone and compact table top model and can be operated using a customized software interface. The design considered a bi-directional chewing motion to enable nearly similar mandible movement pattern as in human. Food texture profile can be estimated using a load cell with capacity up to 300 N. This design included a section of real shaped teeth assembly consisting of three teeth; and a controlled supply line for multi-point saliva injections. The device is fitted with easily replaceable sensors for in situ measurements of conductivity, pH, and temperature. Operating volume of the device can be kept in equivalence with the volume of human oral and nasal space. The device chamber can be hermetically sealed and temperature controlled. A duct system is fitted to connect the device with external analytical systems, such as electronic nose, for measuring gaseous substance release during experimentation. The system also enables easy retrieval of the processed sample so as to use the masticated samples and processed saliva for subsequent analysis by analytical instruments, such as electronic tongue, to identify released soluble compounds and taste profiles. Moreover, the design emphasized on easy cleaning and maintainability. Based on the proposed design, two working prototypes are developed. It is envisaged that the device will be a novel contribution to the progress in the field of food science, new product development, training to future professionals, and strengthening industry-academic collaborations in foreseeable future.

本文介绍了一种用于食品口腔加工研究的机电系统的综合设计方法。所提出的定制设计和原型设备是一个独立的紧凑型桌面模型,可通过定制的软件界面进行操作。设计考虑了双向咀嚼运动,使下颌骨运动模式与人类几乎相似。该设计包括一个由三颗牙齿组成的真实形状的牙齿组件部分;以及一条用于多点唾液注射的受控供应线。该装置安装有易于更换的传感器,用于现场测量电导率、pH 值和温度。设备的工作容积可保持与人体口腔和鼻腔容积相当。设备腔体可以密封并进行温度控制。装置配有一个导管系统,用于连接装置与外部分析系统(如电子鼻),以测量实验过程中释放的气体物质。该系统还便于回收处理过的样本,以便将咀嚼过的样本和处理过的唾液用于电子舌等分析仪器的后续分析,以确定释放的可溶性化合物和味道特征。此外,设计还强调了易于清洁和维护。根据建议的设计,开发了两个工作原型。预计在可预见的未来,该装置将为食品科学领域的进步、新产品开发、未来专业人员培训以及加强产学合作做出新的贡献。
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引用次数: 0
Experimental ginger drying by a novel mixed-mode vertical solar dryer under partial and fully loaded conditions 新型混合模式立式太阳能干燥机在部分和全负荷条件下的生姜干燥实验
IF 6.3 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-07-01 DOI: 10.1016/j.ifset.2024.103736
Amit Malik, Mahesh Kumar

An innovative and compact mixed-mode vertical solar dryer (MVSD) with a circular solar collector is developed and tested for ginger slices drying under partial and fully loaded conditions. Ginger slices samples of 4, 5 and 6 mm thick were used for natural convective drying in MVSD under partially loaded condition. The thickness of the ginger slices was observed to affect the performance of the MVSD. The drying rate and thermal efficiency were observed to be highest for 5 mm thick ginger slices sample under partially loaded condition. The MVSD was further tested with full loading capacity for 5 mm thick ginger slices drying under natural and forced convection modes (NC and FC modes). The drying behavior of ginger slices was well described by Midilli-Kucuk model. Heat transfer coefficients and efficiency (thermal and exergy) were observed to be higher under forced convection mode. Embodied energy and energy payback time were observed as 554.44 and 585.53 kWh; and 2.85 and 2.99 years under NC and FC modes, respectively. The values of annualized capital cost and payback period were observed as INR 389.41 and 408.17; and 1.85 and 6.86 years under NC and FC modes, respectively. The quality of the ginger dried under FC mode was found comparatively better than that of under NC mode.

本研究开发了一种创新的紧凑型混合模式立式太阳能干燥器(MVSD),该干燥器配有一个圆形太阳能集热器,用于在部分和完全负载条件下干燥生姜片。厚度分别为 4、5 和 6 毫米的姜片样品在部分负载条件下在 MVSD 中进行自然对流干燥。据观察,姜片的厚度会影响 MVSD 的性能。在部分负载条件下,厚度为 5 毫米的姜片样品的干燥速率和热效率最高。在自然对流和强制对流模式(NC 和 FC 模式)下,对 5 毫米厚的生姜片进行了全负载能力的 MVSD 进一步测试。Midilli-Kucuk 模型很好地描述了姜片的干燥行为。据观察,强制对流模式下的传热系数和效率(热能和放能)较高。在 NC 和 FC 模式下,体现能耗和能源回收期分别为 554.44 千瓦时和 585.53 千瓦时,以及 2.85 年和 2.99 年。在 NC 和 FC 模式下,年化资本成本和投资回收期分别为 389.41 和 408.17 印度卢比,以及 1.85 和 6.86 年。在 FC 模式下烘干的生姜质量相对优于 NC 模式。
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引用次数: 0
Unconventional technologies as a strategy to improve the phenolic and antioxidant potential of zucchini products enriched with blueberry juice 采用非常规技术提高蓝莓汁西葫芦产品的酚和抗氧化潜力
IF 6.3 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-07-01 DOI: 10.1016/j.ifset.2024.103738
Siluana Katia Tischer Seraglio, Luis Gonzalez-Cavieres, Guido Trautmann-Saez, Constanza Pavez-Guajardo, Jorge Moreno

In this study, unconventional technologies were used to enhance the phenolic and antioxidant content of zucchini pieces by enriching them with blueberry juice. Our results indicated that ohmic heating (OH) increased the extraction rates of compounds with antioxidant potential in blueberry juice, mainly at 70 °C for 15 min and 7.8 V cm1. Furthermore, OH applied after vacuum impregnation led to higher retention rates of phenolic compounds and antioxidant capacity in zucchini pieces impregnated with blueberry juice, especially at 70 °C for 30 min and 7.8 V cm‐−1. The impregnation process also promoted the darkening of zucchini pieces (due to anthocyanin retention) and increased soluble solids. After drying by hot air and vacuum microwave, the phenolic content, antioxidant capacity, physicochemical and color characteristics of the impregnated and non-impregnated zucchinis were distinctly altered. However, vacuum microwave drying at 120 and 460 W can be suggested as the most suitable conditions for both zucchini products, as it resulted in high concentrations of individual phenolic compounds (e.g. up to 44.25, 8.15, and 2.56 mg 100 g‐−1 dry weight (DW) for catechin, gallic acid, and cyanidin, respectively), as well as total phenolic content of up to 484.37 mg gallic acid equivalent 100 g1 DW, total flavonoid content of up to 197.69 mg catechin equivalent 100 g‐−1 DW, and total monomeric anthocyanins of up to 9.48 mg cyanidin 3-glucosideo equivalent 100 g‐−1 DW.

在这项研究中,我们采用了非常规技术,通过在西葫芦中添加蓝莓汁来提高其酚类物质和抗氧化剂的含量。结果表明,欧姆加热(OH)提高了蓝莓汁中具有抗氧化潜力的化合物的萃取率,主要是在 70 °C 15 分钟和 7.8 V cm1 的条件下。此外,在真空浸渍后进行欧姆加热可提高浸渍蓝莓汁的西葫芦片中酚类化合物的保留率和抗氧化能力,尤其是在 70 °C 30 分钟和 7.8 V cm-1 的条件下。浸渍过程还促进了西葫芦片颜色的加深(由于花青素的保留),并增加了可溶性固形物。经过热空气和真空微波干燥后,浸渍和未浸渍西葫芦的酚含量、抗氧化能力、理化和颜色特征都发生了明显变化。不过,120 瓦和 460 瓦的真空微波干燥对这两种西葫芦产品来说都是最合适的条件,因为它能产生高浓度的单个酚类化合物(例如,高达 44.25、8.15 和 2.56 毫克 100 克-1 干重(DW)),总酚含量高达 484.37 毫克没食子酸当量(100 克-1 干重),总类黄酮含量高达 197.69 毫克儿茶素当量(100 克-1 干重),单体花青素总量高达 9.48 毫克青花素-3-葡萄糖当量(100 克-1 干重)。
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引用次数: 0
Improving dried mango physicochemical properties using conventional hot-air drying coupled with a novel technology “intensification of vaporization by decompression to the vacuum” 利用传统热风干燥技术和 "通过减压至真空加强汽化 "的新技术改善芒果干的理化特性
IF 6.3 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-07-01 DOI: 10.1016/j.ifset.2024.103739
Paola Labaky , Layal Dahdouh , Lidwine Grosmaire , Hiba N. Rajha , Julien Ricci , Charlotte Delpech , André El Khoury , Espérance Debs , Christelle Wisniewski , Nicolas Louka

The impact of the “Intensification of Vaporization by Decompression to the Vacuum” (IVDV) coupled with conventional hot-air drying on the organoleptic and nutritional properties of mangoes was investigated in this study. The effect of three IVDV treatment parameters (saturated steam pressure, initial water content and processing time) on the volume, texture and color was studied using response surface methodology. The phenolic content and antioxidant activity were explored through chemical analyses. Results revealed that the IVDV decreased the drying time of mango cubes by 50%, increased their volume by four times, and improved their texture compared to hot-air dried samples. The treatment also enhanced the color of mango cubes allowing an orange color contrasted to a brown color for conventionally dried cubes. Phenolic content and antioxidant activities were improved by 9 times and 11 times, respectively, following IVDV treatment compared to simple hot-air drying. The IVDV offers new prospects for processing mango into dried cubes with improved organoleptic properties characterized by a crunchy texture and an appreciated color.

本研究调查了 "减压至真空强化蒸发"(IVDV)与传统热风干燥对芒果感官和营养特性的影响。采用响应面方法研究了三个 IVDV 处理参数(饱和蒸汽压、初始含水量和处理时间)对体积、质地和颜色的影响。通过化学分析探讨了酚含量和抗氧化活性。结果表明,与热风干燥样品相比,IVDV 使芒果块的干燥时间缩短了 50%,体积增加了四倍,质地得到改善。这种处理方法还提高了芒果块的色泽,使其呈现橙色,而传统干燥的芒果块则呈现棕色。与简单的热风干燥相比,IVDV 处理后的酚含量和抗氧化活性分别提高了 9 倍和 11 倍。IVDV 为将芒果加工成具有更好感官特性的干果块提供了新的前景,其特点是口感松脆,颜色悦目。
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引用次数: 0
Techno-functional properties of Camelina sativa cake proteins treated with the instant controlled pressure drop (DIC) technology 瞬时可控压降(DIC)技术处理的荠菜饼蛋白的技术功能特性
IF 6.3 1区 农林科学 Q1 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-07-01 DOI: 10.1016/j.ifset.2024.103741
Mario Adrian Tienda-Vazquez , Mariana Perez-Herrera , Oscar Carrasco-Morales , Carmen Tellez-Perez , Maritza Alonzo-Macias , Anaberta Cardador-Martínez

The instant controlled pressure drop (DIC) is one of the emerging technologies in food that can affect the extraction and techno-functional properties of proteins. Camelina sativa cake was subjected to various DIC treatments, with pressure (0.2–0.7 MPa) and exposure time (20–60 s) variables. Afterwards, protein extraction was conducted, and the influence of individual or combined variables on the techno-functional properties of the protein concentrate was analyzed, and each treatment was later analyzed against the control. Furthermore, DIC increased the protein extraction yield. The pressure, time, and their interaction variables influenced the oil absorption capacity (OAC), foaming capacity (FC), and stability (FS), while water-holding capacity (WHC) was solely affected by pressure. The results of comparing DIC against control showed significant differences in OAC, emulsifying activity index (EAI), FS, and FC. These findings strongly indicate that DIC enhances protein extraction yield and modifies the techno-functional properties of camelina proteins.

瞬时可控压降(DIC)是食品领域的新兴技术之一,可影响蛋白质的提取和技术功能特性。对荠菜饼进行了不同的 DIC 处理,压力(0.2-0.7 兆帕)和暴露时间(20-60 秒)均可变。然后,进行蛋白质提取,分析单个变量或组合变量对浓缩蛋白质的技术功能特性的影响,并将每种处理方法与对照组进行对比分析。此外,DIC 提高了蛋白质提取率。压力、时间及其交互变量影响吸油能力(OAC)、发泡能力(FC)和稳定性(FS),而持水能力(WHC)仅受压力影响。DIC 与对照组的比较结果表明,两者在 OAC、乳化活性指数(EAI)、FS 和 FC 方面存在显著差异。这些发现有力地表明,DIC 提高了蛋白质提取率,并改变了荠菜蛋白质的技术功能特性。
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引用次数: 0
Eggshell membrane as a natural food-grade scaffold for cultured meat 蛋壳膜作为培养肉的天然食品级支架
IF 6.6 1区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-06-16 DOI: 10.1016/j.ifset.2024.103734
Si Won Jang , Jae Ho Han , Ye Rim Kim , Hoon Jang , Kwan Seob Shim , Hyun Woo Choi

The increasing global population and growing necessity for sustainable food production, cultured meat production has emerged as a promising technology. However, its successful production requires edible food-grade scaffolds and reduced production costs. In this study we determined the feasibility of eggshell membrane (ESM) as a natural food-grade scaffold. We optimized an efficient ESM extraction method and storage temperature with high cell attachment efficiency. We assessed the maintenance, differentiation and proliferation of bMuSCs on culture dish and ESM. As a result, it was confirmed that maintenance, differentiation, and proliferation markers were higher on ESM than culture dish. Finally, we determined 1 ng/ml of bFGF and 5% horse serum (HS) concentrations for optimal maintenance and differentiation of bMuSCs on ESM. Based on this, after long-term culture, the ESM scaffold supported the bovine myotube differentiation. Ultimately, ESM is shown to be a valuable scaffold biomaterial with a role to play in the production of cultured meat.

Industrial relevance

This research used by-product of egg, a natural food-grade raw material, as a scaffold for cultured meat production. By upcycling, wasted and broken eggshells from industry materials, the approach is environmentally friendly. Egg membranes are convenient for food processing and long-term storage, safe to consume in terms of food safety, and can be supplied continuously at a low cost. In the production of cultured meat, it is necessary to use eggshell membranes with microbial loads that are strictly controlled throughout the processes of separation, storage, and usage. This experiment demonstrated that eggshell membranes exhibit high proliferation, differentiation, and adhesion efficiency in bovine muscle stem cell culture, proving that cultured meat can be produced with high efficiency and low cost at the production stage.

随着全球人口的不断增长和对可持续食品生产需求的不断增加,养殖肉类生产已成为一项前景广阔的技术。然而,要成功生产培养肉,就必须采用可食用的食品级支架并降低生产成本。在本研究中,我们确定了蛋壳膜(ESM)作为天然食品级支架的可行性。我们优化了ESM的提取方法和储存温度,使其具有较高的细胞附着效率。我们评估了bMuSCs在培养皿和ESM上的维持、分化和增殖情况。结果证实,ESM上的维持、分化和增殖指标均高于培养皿。最后,我们确定了 1 纳克/毫升的 bFGF 和 5%的马血清(HS)浓度为 bMuSCs 在 ESM 上的最佳维持和分化浓度。在此基础上,经过长期培养,ESM支架支持了牛肌管的分化。最终,ESM 被证明是一种有价值的支架生物材料,可在培养肉的生产中发挥作用。通过对工业原料中的废弃蛋壳和破损蛋壳进行升级再利用,该方法非常环保。蛋膜便于食品加工和长期储存,在食品安全方面可放心食用,而且可持续供应,成本低廉。在养殖肉类的生产中,有必要使用在分离、储存和使用的整个过程中都严格控制微生物负荷的蛋壳膜。该实验证明,蛋壳膜在牛肌肉干细胞培养中表现出较高的增殖、分化和粘附效率,证明在生产阶段可以高效率、低成本地生产培养肉。
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引用次数: 0
Understanding the evolution of moisture during isothermal dehydration of glutinous rice through global sensitivity analysis 通过全局敏感性分析了解糯米等温脱水过程中的水分变化
IF 6.6 1区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-06-15 DOI: 10.1016/j.ifset.2024.103733
Kabiru Ayobami Jimoh , Norhashila Hashim , Rosnah Shamsudin , Hasfalina Che Man , Mahirah Jahari , Renny Eka Putri

This study examined the effect of layer thickness and temperature on the evolution of moisture during the isothermal dehydration of glutinous rice. To analyse the moisture evolution, empirical models and secondary models (SM) were employed. Global sensitivity analysis (GSA) was used to estimate the importance of the experimental parameters on the developed SM. According to the dehydration curves, the increase in temperature and reduction in the layer thickness significantly shortened (P<0.05) the dehydration time of glutinous rice. The effective diffusivity, activation energy, and Gibb-free energy were 2.0×1012m2/s to 2.53×1011m2/s, 43.03 kJmol1 to 51.05 kJmol1, and 145.10 kJmol1 to 155.85 kJmol1respectively. The Page and Logarithmic models are suitably considered in evaluating the dehydration kinetics of the glutinous rice with a high coefficient of determination (R2) values of >0.9989. The SM aptly described moisture evolution with higher accuracy of R2=0.9843. The GSA shows that the variation in the SM output is primarily driven by the variation in the input parameters with low reliance on its interaction with other parameters, indicating that the SM can play a significant role in the optimization of the industrial dehydration process with a wide range of applications in the agricultural production system.

本研究探讨了糯米等温脱水过程中层厚度和温度对水分演变的影响。为分析水分演变,采用了经验模型和二级模型(SM)。全局敏感性分析(GSA)用于估算实验参数对所建立的二级模型的重要性。根据脱水曲线,温度的升高和层厚度的减小显著缩短了糯米的脱水时间(P<0.05)。有效扩散率、活化能和无吉布能分别为 2.0×10-12m2/s 至 2.53×10-11m2/s、43.03 kJmol-1 至 51.05 kJmol-1 和 145.10 kJmol-1 至 155.85 kJmol-1。在评估糯米的脱水动力学时,佩奇模型和对数模型得到了适当的考虑,其决定系数 (R2) 高达 >0.9989。SM模型以R2=0.9843的较高精确度恰当地描述了水分的变化。GSA 表明,SM 输出的变化主要由输入参数的变化驱动,对其与其他参数的相互作用依赖性较低,这表明 SM 在优化工业脱水过程中可发挥重要作用,在农业生产系统中具有广泛的应用前景。
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引用次数: 0
Evaluation of strain variability of food microorganisms in response to decontamination by pulsed electric fields and thermal treatments 评估食品微生物菌株在脉冲电场和热处理去污过程中的变异性
IF 6.3 1区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-06-13 DOI: 10.1016/j.ifset.2024.103731
Fotios Lytras , Georgios Psakis , Ruben Gatt , Joerg Hummerjohann , Javier Raso , Vasilis Valdramidis

The effect of pulsed electric fields (PEF) and thermal treatments on the inactivation of the population of 40 strains of 4 model microorganisms (Escherichia coli, Listeria monocytogenes, Lactiplantibacillus plantarum, Saccharomyces cerevisiae) were investigated. Microbial samples of McIlvaine buffer pH 7.0 were subjected to pulses with electric field strength 20 kV/cm and total specific energies (88, 136, and 184 kJ/kg). Depending on the species and strain, microorganisms exhibited various resistances. PEF microbial resistance and strain variability data were correlated to the total specific energy used. E. coli strains showed statistical log10 inactivation differences under the 88 and 136 kJ/kg but not under the 184 kJ/kg PEF treatment. In contrast, L. monocytogenes strains showed statistical log10 inactivation differences only under the 184 kJ/kg treatment. L. monocytogenes L6 strain was identified as the most resistant strain at PEF treatment (184 kJ/kg). This result was in accordance with the resistance under thermal treatment (62.8 °C, 30 min).

Industrial relevance

The identification of target microorganisms related to their resistance in one or more technologies can help at establishing treatment conditions that reassure food safety. Data obtained in this research show that species and strain behaviours vary and are dependent on the technology and the applied treatment conditions. Thus, the resistance exhibited by microorganisms of public health importance may be dependent on the used technology and the applied treatment.

研究了脉冲电场(PEF)和热处理对 4 种模式微生物(大肠杆菌、单核细胞增生李斯特菌、植物乳杆菌和酿酒酵母菌)40 株菌群灭活率的影响。对 pH 值为 7.0 的 McIlvaine 缓冲液中的微生物样本施加电场强度为 20 kV/cm、总比能量为 88、136 和 184 kJ/kg 的脉冲。根据种类和菌株的不同,微生物表现出不同的抗性。PEF 微生物抗性和菌株变异数据与所使用的总比能量相关。大肠杆菌菌株在 88 和 136 千焦/千克的 PEF 处理下显示出统计学上的 log10 灭活差异,而在 184 千焦/千克的 PEF 处理下则没有。相比之下,单核细胞增生 L. 菌株只有在 184 kJ/kg 处理条件下才显示出统计学对数 10 的灭活差异。在 PEF 处理(184 kJ/kg)下,单核细胞增多性酵母菌 L6 菌株被确定为抗性最强的菌株。这一结果与热处理(62.8 °C,30 分钟)下的抗性相一致。工业相关性识别目标微生物对一种或多种技术的抗性有助于建立确保食品安全的处理条件。这项研究获得的数据表明,物种和菌株的行为各不相同,并取决于所采用的技术和处理条件。因此,对公共卫生具有重要意义的微生物所表现出的抗药性可能取决于所使用的技术和应用的处理方法。
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引用次数: 0
Surface properties and antibacterial characteristics of polyurethane modified by corona discharge for food processing industry 用于食品加工业的电晕放电改性聚氨酯的表面性能和抗菌特性
IF 6.6 1区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-06-08 DOI: 10.1016/j.ifset.2024.103729
E.C. Stancu , M.D. Ionita , A. Quade , E.R. Ionita

Thermal properties and durability make polyurethane (PU) ideal for conveyor belts in food processing industry. On the other hand, its susceptibility to adhesion of pathogens subjects him to surface treatment techniques. In this study, substrates of PU were exposed to corona discharge using air as treatment gas. The process parameters, such as treatment time and nozzle-substrate distance, and the microbicidal effects of the polymer surfaces against Staphylococcus aureus and Escherichia coli were examined. Changes in surface hydrophobicity occurred at short treatment times due to the introduction of polar groups, as proofed by X-ray Photoelectron Spectroscopy (XPS), while the surface morphology suffered minor changes as revealed by Scanning Electron Microscopy (SEM) imaging. Moreover, the hydrophilicity of plasma treated PU was minimal affected by the variation of nozzle-substrate distance, as long as the discharge was in contact with the polymer surface. The hydrophilic surfaces developed a very good resistance to bacteria adherence in few hours after incubation.

聚氨酯(PU)的热性能和耐用性使其成为食品加工业传送带的理想材料。另一方面,聚氨酯容易粘附病原体,因此需要采用表面处理技术。在这项研究中,使用空气作为处理气体,对聚氨酯基材进行电晕放电。研究了处理时间、喷嘴与基底的距离等工艺参数,以及聚合物表面对金黄色葡萄球菌和大肠杆菌的杀菌效果。X 射线光电子能谱(XPS)证明,在短处理时间内,由于极性基团的引入,表面疏水性发生了变化,而扫描电子显微镜(SEM)成像显示,表面形态发生了轻微变化。此外,只要放电与聚合物表面接触,经过等离子处理的聚氨酯的亲水性受喷嘴与基底距离变化的影响很小。亲水性表面在培养几小时后就能很好地抵抗细菌的附着。
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Innovative Food Science & Emerging Technologies
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