Multisensor Magnetic Scanning Microscope for Remanent Magnetic Field Measurements

João F. Chaves, L. F. Noris, E. Yokoyama, F. Osorio G., Leonardo A. F. Mendoza, J. F. Araujo
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Abstract

Magnetic Scanning Microscopy (MSM) emerged with the aim of allowing the visualization of magnetic fields of a sample or material through scanning and proved particularly useful for geology, biomedicine, characterization of magnetic materials, and in the steel industry. In this regard, the reading system of an MSM was modified using a μ-metal magnetic shielding structure to analyze remanent fields. The MSM was adapted to perform readings using two different types of sensors. The sensitive area of the sensors was evaluated, and the HQ-0811 (AKM—Asahi KaseiTM Microdevices) and STJ-010 (Micro MagneticsTM) sensors were chosen, with the HQ-0811 standardized on Printed Circuit Boards (PCBs) to facilitate handling and increase the system’s robustness. In the shielded chamber, two piezoelectric ANC-150 stepper motors (Attocube Systems) were used, arranged planarly, to allow the movement of the analyzed samples under the mounted sensors. To acquire data from the sensors, the Precision Current Source Model 6220 and the Nanovoltmeter Model 2182A (both from Keithley) were used, along with Keithley’s Delta-Mode integrated system. To analyze the system’s effectiveness, three distinct samples were analyzed for calibration, and a MATLAB program was written to analyze the images and extract the material’s magnetization. Additionally, a rock sample from the Parnaíba Basin was mapped to demonstrate the system’s capabilities.
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用于残余磁场测量的多传感器磁扫描显微镜
磁扫描显微镜(MSM)的出现旨在通过扫描实现样品或材料磁场的可视化,在地质学、生物医学、磁性材料表征和钢铁工业中被证明特别有用。为此,对 MSM 的读取系统进行了改进,使用了 μ 金属磁屏蔽结构来分析剩磁磁场。MSM 经改装后可使用两种不同类型的传感器进行读数。对传感器的敏感区域进行了评估,最终选择了 HQ-0811 (AKM-Asahi KaseiTM Microdevices)和 STJ-010 (Micro MagneticsTM)传感器,其中 HQ-0811 采用标准化印刷电路板 (PCB),以方便处理并提高系统的坚固性。在屏蔽室中,使用了两个压电式 ANC-150 步进电机(Attocube 系统公司),它们呈平面排列,以便在安装的传感器下移动分析样品。为了从传感器获取数据,使用了 6220 型精密电流源和 2182A 型纳米伏特计(均来自吉时利)以及吉时利的 Delta-Mode 集成系统。为了分析系统的有效性,对三个不同的样本进行了校准分析,并编写了 MATLAB 程序来分析图像并提取材料的磁化率。此外,还对来自帕尔奈巴盆地的岩石样本进行了测绘,以展示该系统的功能。
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