Effect of the Spark-Plasma-Sintering Temperature on the Structure, Crystallographic Texture, and Thermoelectric Properties of Materials Based on One-Dimensional Particles of Bi2Te2.7Se0.3

IF 0.8 Q3 Engineering Nanotechnologies in Russia Pub Date : 2024-03-21 DOI:10.1134/S2635167623600992
M. N. Yapryntsev, O. N. Ivanov
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Abstract

In this work we obtain and certify one-dimensional particles of the composition Bi2Te2.7Se0.3 of submicron size with an atypical growth direction. Further, the influence of the temperature of spark plasma sintering on the grain morphology and size, crystal-lattice parameters, elemental composition, and density of the samples obtained are investigated. The features of the formation of the crystallographic texture depending on the sintering temperature are also established. A temperature is revealed that allows for preservation of the crystal structure characteristic of the initial powder and materials with an atypical crystallographic texture to obtained. The thermoelectric properties of the materials obtained are also studied.

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火花等离子烧结温度对基于 Bi2Te2.7Se0.3 一维颗粒的材料的结构、晶体纹理和热电性能的影响
摘要 在这项工作中,我们获得并验证了成分为 Bi2Te2.7Se0.3、具有非典型生长方向的亚微米级一维颗粒。此外,还研究了火花等离子体烧结温度对所获样品的晶粒形态和尺寸、晶格参数、元素组成和密度的影响。此外,还确定了根据烧结温度形成晶体纹理的特征。结果表明,烧结温度既能保持初始粉末的晶体结构特征,又能获得具有非典型晶体纹理的材料。此外,还研究了所获材料的热电特性。
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来源期刊
Nanotechnologies in Russia
Nanotechnologies in Russia NANOSCIENCE & NANOTECHNOLOGY-
CiteScore
1.20
自引率
0.00%
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0
期刊介绍: Nanobiotechnology Reports publishes interdisciplinary research articles on fundamental aspects of the structure and properties of nanoscale objects and nanomaterials, polymeric and bioorganic molecules, and supramolecular and biohybrid complexes, as well as articles that discuss technologies for their preparation and processing, and practical implementation of products, devices, and nature-like systems based on them. The journal publishes original articles and reviews that meet the highest scientific quality standards in the following areas of science and technology studies: self-organizing structures and nanoassemblies; nanostructures, including nanotubes; functional and structural nanomaterials; polymeric, bioorganic, and hybrid nanomaterials; devices and products based on nanomaterials and nanotechnology; nanobiology and genetics, and omics technologies; nanobiomedicine and nanopharmaceutics; nanoelectronics and neuromorphic computing systems; neurocognitive systems and technologies; nanophotonics; natural science methods in a study of cultural heritage items; metrology, standardization, and monitoring in nanotechnology.
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