Computational and Experimental Study of the Mechanical Properties of Porous Particles Based on Cellulose Diacetate

IF 0.8 Q3 Engineering Nanotechnologies in Russia Pub Date : 2024-03-21 DOI:10.1134/S2635167623600785
O. V. Nikulenkova, A. E. Krupnin, Yu. D. Zagoskin, S. N. Malakhov, N. M. Kuznetsov, S. N. Chvalun
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Abstract

The mechanical behavior of porous particles of various diameters obtained by the cryolyophilization drying of frozen droplets of 1-wt % cellulose diacetate solution in 1,4-dioxane are studied. The morphology of the particles is visualized by scanning electron microscopy. It is shown that the particles have a predominantly spherical shape and a branched porous structure. The elastic and tangent moduli, Poisson’s ratio, and yield strength of the particle material are determined through mechanical tests of individual particles compressed between parallel plates. The results are then used to solve the reverse-engineering problem using the finite-element method. A bilinear stress-strain diagram taking into account the plastic properties of the particle material is obtained. Verification of the obtained model was carried out in a similar experiment upon the compression of particles of a different diameter.

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基于二醋酸纤维素的多孔颗粒力学性能的计算与实验研究
研究了通过冷冻干燥 1-wt % 二醋酸纤维素溶液在 1,4-dioxane 中的冷冻液滴而获得的不同直径的多孔颗粒的机械行为。通过扫描电子显微镜观察了颗粒的形态。结果表明,这些颗粒主要呈球形,并具有多孔分支结构。通过对压缩在平行板之间的单个颗粒进行机械测试,确定了颗粒材料的弹性模量、切线模量、泊松比和屈服强度。然后使用有限元法解决逆向工程问题。得到的双线性应力应变图考虑了颗粒材料的塑性特性。在压缩不同直径颗粒的类似实验中对所获得的模型进行了验证。
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来源期刊
Nanotechnologies in Russia
Nanotechnologies in Russia NANOSCIENCE & NANOTECHNOLOGY-
CiteScore
1.20
自引率
0.00%
发文量
0
期刊介绍: Nanobiotechnology Reports publishes interdisciplinary research articles on fundamental aspects of the structure and properties of nanoscale objects and nanomaterials, polymeric and bioorganic molecules, and supramolecular and biohybrid complexes, as well as articles that discuss technologies for their preparation and processing, and practical implementation of products, devices, and nature-like systems based on them. The journal publishes original articles and reviews that meet the highest scientific quality standards in the following areas of science and technology studies: self-organizing structures and nanoassemblies; nanostructures, including nanotubes; functional and structural nanomaterials; polymeric, bioorganic, and hybrid nanomaterials; devices and products based on nanomaterials and nanotechnology; nanobiology and genetics, and omics technologies; nanobiomedicine and nanopharmaceutics; nanoelectronics and neuromorphic computing systems; neurocognitive systems and technologies; nanophotonics; natural science methods in a study of cultural heritage items; metrology, standardization, and monitoring in nanotechnology.
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