Synthesis of Material Composite rGO-TIO2 From Coconut Shells by Sol-Gel Methods as Photocatalyst

U. Hikmah, Diah Risma Yanti, David Lee Giant Axala
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Abstract

The rGO- TiO2 composite photocatalyst is receiving great attention because of its high performance. But the study of rGO- TiO2 composite with sources of rGO material derived from the utilization of organic waste such as coconut shells is limited. In this study, the synthesis of nanocomposite rGO- TiO2 was described with rGO obtained from coconut shells. The rGO samples produce through the oxidation and reduction process. The transformation of graphene oxide into reduced graphene oxide was assisted by microwave irradiation. The obtained rGO was then composite with Titanium tetraisopropoxide (TTIP) by the sol-gel method. The composite of rGO- TiO2 was characterized by XRD, FTIR, UV-Vis, and SEM. The photocatalytic performance of the rGO- TiO2 composite was conducted on Methylene blue. The result shows that rGO- TiO2composite has a good photocatalytic performance with the highest number at 96%.
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用溶胶-凝胶法从椰子壳中合成作为光催化剂的 rGO-TIO2 复合材料
rGO- TiO2 复合光催化剂因其高性能而备受关注。但利用从椰壳等有机废物中提取的 rGO 材料进行 rGO- TiO2 复合材料的研究还很有限。本研究介绍了利用从椰子壳中获得的 rGO 合成纳米复合材料 rGO- TiO2 的方法。rGO 样品通过氧化和还原过程产生。氧化石墨烯在微波辐照下转化为还原氧化石墨烯。然后用溶胶-凝胶法将得到的 rGO 与四异丙醇钛(TTIP)复合。通过 XRD、FTIR、UV-Vis 和 SEM 对 rGO- TiO2 的复合材料进行了表征。对 rGO- TiO2 复合材料在亚甲基蓝上的光催化性能进行了研究。结果表明,rGO- TiO2 复合材料具有良好的光催化性能,最高光催化活性达到 96%。
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