The influence of hygroscopic expansion of resin supporting dies on the fracture resistance of ceramic restorations during thermal cycling

IF 4.6 1区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Dental Materials Pub Date : 2024-06-08 DOI:10.1016/j.dental.2024.06.011
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Abstract

Objectives

To evaluate the hygroscopic expansion characterization of resin composite dies during thermal cycling, and their influence on the fracture resistance of dental ceramic materials as well as the effect of pre-immersion on these measurements.

Methods

Disc-shaped specimens (φ = 15.0 mm, h = 1.2 mm) and anatomical crown dies of four resin composites (epoxy, Z350, P60, G10) were fabricated. Disc-shaped samples were continuously soaked in distilled water and the volume expansion was measured at different time point by Archimedes method. Disc-shaped samples were pre-immersed for 0, 7, or 30 days, elastic modulus and hardness were measured using Nanoindentation test; thermal cycling (TC) test was performed (5 °C-55 °C, 104 cycles), and volume expansion during TC was measured. Four kinds of resin die with pre-immersion for 0, 7, or 30 days were cemented to 5Y-Z crown, or epoxy dies without pre-immersion were cemented to 5Y-Z, 3Y-Z and lithium disilicate glass (LDG) crowns, and load-to-failure testing was performed before and after TC. Finite element analysis (FEA) and fractography analysis were also conducted.

Results

The hygroscopic expansion was in the order: epoxy > Z350 > P60 > G10. Except for G10, the other three resin composites exhibited different degrees of hygroscopic expansion during TC. Only the elastic modulus and hardness of epoxy decreased after water storage. However, only the fracture loads of 5Y-Z and LDG crowns supported by epoxy dies were significantly decreased after TC. FEA showed a stress concentration at the cervical region of the crown after volume expansion of the die, leading to the increase of the peak stress at the crown during loading.

Significance: Only the hygroscopic expansion of epoxy dies caused by TC led to the decrease in the fracture resistance of the 5Y-Z and LDG crown, which may be related to the decrease in the elastic modulus of the epoxy die and the tensile stress caused by it.

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热循环过程中树脂支撑模的吸湿膨胀对陶瓷修复体抗折性的影响。
目的评估树脂复合材料模具在热循环过程中的吸湿膨胀特性及其对牙科陶瓷材料抗断裂性能的影响,以及预浸泡对这些测量的影响:方法:制作了四种树脂复合材料(环氧树脂、Z350、P60 和 G10)的圆盘状试样(φ = 15.0 毫米,h = 1.2 毫米)和解剖冠模。将圆盘状样品连续浸泡在蒸馏水中,用阿基米德法测量不同时间点的体积膨胀率。圆盘状样品预浸 0、7 或 30 天,使用纳米压痕测试测量弹性模量和硬度;进行热循环(TC)测试(5 ℃-55 ℃,104 次循环),测量热循环期间的体积膨胀率。将预浸 0 天、7 天或 30 天的四种树脂模具粘结到 5Y-Z 牙冠上,或将未预浸泡的环氧树脂模具粘结到 5Y-Z、3Y-Z 和二硅酸锂玻璃(LDG)牙冠上,并在热循环之前和之后进行加载至破坏测试。同时还进行了有限元分析(FEA)和断裂分析:吸湿膨胀的顺序为:环氧树脂 > Z350 > P60 > G10。除 G10 外,其他三种树脂复合材料在 TC 期间均表现出不同程度的吸湿膨胀。只有环氧树脂的弹性模量和硬度在贮水后有所下降。然而,只有环氧树脂模具支撑的 5Y-Z 和 LDG 牙冠的断裂载荷在 TC 后明显降低。有限元分析表明,模具体积膨胀后,牙冠颈部应力集中,导致加载时牙冠处的峰值应力增加:只有 TC 引起的环氧树脂模具吸湿膨胀才会导致 5Y-Z 和 LDG 牙冠的抗断裂性降低,这可能与环氧树脂模具的弹性模量降低及其引起的拉应力有关。
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来源期刊
Dental Materials
Dental Materials 工程技术-材料科学:生物材料
CiteScore
9.80
自引率
10.00%
发文量
290
审稿时长
67 days
期刊介绍: Dental Materials publishes original research, review articles, and short communications. Academy of Dental Materials members click here to register for free access to Dental Materials online. The principal aim of Dental Materials is to promote rapid communication of scientific information between academia, industry, and the dental practitioner. Original Manuscripts on clinical and laboratory research of basic and applied character which focus on the properties or performance of dental materials or the reaction of host tissues to materials are given priority publication. Other acceptable topics include application technology in clinical dentistry and dental laboratory technology. Comprehensive reviews and editorial commentaries on pertinent subjects will be considered.
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