Evaluation of the tensile strength and impact property of polyamide/short glass fibre-multi-walled carbon nanotube composites: an experimental study based on response surface method

Simin Ahmadi, Hassan Abdoos, Ehsan Borhani, Alireza Albooyeh
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Abstract

The tensile strength, impact property and thermal stability of polyamide 6 (PA6) reinforced with carboxylic acid-functionalised multi-walled carbon nanotubes (MWCNTs) with 1 and 2 wt.%, and short glass fibre (SGF) with 10 and 20 wt.%, were investigated. The morphological properties were examined by SEM. The differential scanning calorimetry (DSC) was also carried out to explore the thermal stability and crystallinity of nanocomposites. For determining the optimal weight percentage of reinforcements, the response surface methodology (RSM) was used. The effect of nanotubes and weight percentages of fibre on the tensile and impact properties was investigated by analysis of variance. The results indicated that the incorporation of MWCNTs to PA6 increased the tensile and impact strength of the matrix by 16% and 24%, respectively. Also, the addition of SGFs to polyamide improved the mechanical properties. The results also showed that the nanocomposite containing 1 wt.% MWCNTs and 20 wt.% SGFs had the highest properties (66% increase for tensile and 81% increase for impact strength compared to neat PA6). The DSC results confirmed the effect of reinforcements on thermal characteristics of nanocomposites. The validation of output models of responses implies the ability of models to predict the tensile and impact behaviour of composites.
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聚酰胺/短玻璃纤维-多壁碳纳米管复合材料的拉伸强度和冲击性能评估:基于响应面法的实验研究
研究了羧酸功能化多壁碳纳米管(MWCNTs)(1 和 2 wt.%)和短玻璃纤维(SGF)(10 和 20 wt.%)增强的聚酰胺 6(PA6)的拉伸强度、冲击性能和热稳定性。扫描电镜对其形态特性进行了检测。此外,还进行了差示扫描量热法(DSC)研究纳米复合材料的热稳定性和结晶度。为确定增强材料的最佳重量百分比,采用了响应面方法(RSM)。通过方差分析研究了纳米管和纤维重量百分比对拉伸和冲击性能的影响。结果表明,在 PA6 中加入 MWCNTs 后,基体的拉伸强度和冲击强度分别提高了 16% 和 24%。此外,在聚酰胺中加入 SGFs 也改善了其机械性能。结果还显示,含有 1 wt.% MWCNTs 和 20 wt.% SGFs 的纳米复合材料具有最高的性能(与纯 PA6 相比,拉伸强度提高了 66%,冲击强度提高了 81%)。DSC 结果证实了增强材料对纳米复合材料热特性的影响。输出响应模型的验证意味着模型能够预测复合材料的拉伸和冲击行为。
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