Nouran Yousri, Hesham H. El-Feky, Mostafa Y. Nassar, Alaa S. Amin
{"title":"Nanoscale Zero-valent Silver and Graphene Oxide Nanoparticles: Facile Synthesis and Characterization","authors":"Nouran Yousri, Hesham H. El-Feky, Mostafa Y. Nassar, Alaa S. Amin","doi":"10.9734/ajocs/2024/v14i3310","DOIUrl":null,"url":null,"abstract":"We herein report a direct and facile hydrothermal method for the preparation of zero-valent silver nanoparticles using a mixture of ascorbic acid/starch as a reducing agent. The average crystallite size of the prepared Ag0 nanoparticles was ca. 46.7 nm. The zero-valent silver nano-products were characterized by using FT-IR, FE-SEM, and XRD analyses. In addition, this work shows an improved synthesis of graphene oxide nanoparticles. The average crystallite size of the prepared graphene-oxide nanoparticles was ca. 6.0nm. The graphene oxide nanoparticles were also characterized by using FT-IR, FE-SEM, and XRD analyses.","PeriodicalId":8505,"journal":{"name":"Asian Journal of Chemical Sciences","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2024-06-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Asian Journal of Chemical Sciences","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.9734/ajocs/2024/v14i3310","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
We herein report a direct and facile hydrothermal method for the preparation of zero-valent silver nanoparticles using a mixture of ascorbic acid/starch as a reducing agent. The average crystallite size of the prepared Ag0 nanoparticles was ca. 46.7 nm. The zero-valent silver nano-products were characterized by using FT-IR, FE-SEM, and XRD analyses. In addition, this work shows an improved synthesis of graphene oxide nanoparticles. The average crystallite size of the prepared graphene-oxide nanoparticles was ca. 6.0nm. The graphene oxide nanoparticles were also characterized by using FT-IR, FE-SEM, and XRD analyses.
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