V. F. Gremenok, N. N. Musaeva, Kh. Kh. Khalilova, A. L. Zheludkevich, O. F. Demidenko, D. A. Kiselev, V. V. Khoroshko, B. M. Izzatov, M. T. Alizade
{"title":"Microstructure and Optical Characteristics of Nickel Nanoparticles Obtained by One-Step Synthesis Method","authors":"V. F. Gremenok, N. N. Musaeva, Kh. Kh. Khalilova, A. L. Zheludkevich, O. F. Demidenko, D. A. Kiselev, V. V. Khoroshko, B. M. Izzatov, M. T. Alizade","doi":"10.1007/s10812-024-01755-3","DOIUrl":null,"url":null,"abstract":"<p>Nickel nanoparticles were synthesized at room temperature by a one-step method of chemical reduction of Ni ions from NiCl<sub>2</sub>∙6H<sub>2</sub>O using NaBH<sub>4</sub>. The microstructure of the nanoparticles was studied by x-ray diffraction, Raman spectroscopy, and scanning and transmission electron microscopy. An analysis of x-ray diffraction and Raman spectroscopy data showed that the obtained nanoparticles had the cubic metallic Ni structure with a crystallite size (coherent scattering region) of 3–6 nm. Studies of the morphology indicated that the Ni nanoparticles were spherical in shape and in contact with each other to form large agglomerates of nanograins.</p>","PeriodicalId":609,"journal":{"name":"Journal of Applied Spectroscopy","volume":"91 3","pages":"570 - 574"},"PeriodicalIF":1.0000,"publicationDate":"2024-07-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Applied Spectroscopy","FirstCategoryId":"92","ListUrlMain":"https://link.springer.com/article/10.1007/s10812-024-01755-3","RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"SPECTROSCOPY","Score":null,"Total":0}
引用次数: 0
Abstract
Nickel nanoparticles were synthesized at room temperature by a one-step method of chemical reduction of Ni ions from NiCl2∙6H2O using NaBH4. The microstructure of the nanoparticles was studied by x-ray diffraction, Raman spectroscopy, and scanning and transmission electron microscopy. An analysis of x-ray diffraction and Raman spectroscopy data showed that the obtained nanoparticles had the cubic metallic Ni structure with a crystallite size (coherent scattering region) of 3–6 nm. Studies of the morphology indicated that the Ni nanoparticles were spherical in shape and in contact with each other to form large agglomerates of nanograins.
期刊介绍：
Journal of Applied Spectroscopy reports on many key applications of spectroscopy in chemistry, physics, metallurgy, and biology. An increasing number of papers focus on the theory of lasers, as well as the tremendous potential for the practical applications of lasers in numerous fields and industries.
京公网安备 11010802042870号
京ICP备2023020795号-1
分享
求助内容：
应助结果提醒方式：
扫码关注我们
