Obtaining coffee mucilage microcapsules by spray drying using chemically modified banana starch

Jenny Ríos-Hernández, Andrés Chávez-Salazar, Erika M. Restrepo-Montoya, F. Castellanos-Galeano, Diana Y. Ospina-López
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Abstract

The growing global consumption of coffee has positioned Colombia as the third largest producer worldwide. However, the processing of coffee beans generates significant by-products, such as mucilage, which is rich in phenolic compounds with antioxidant activity. Inadequate disposal of this waste creates environmental problems and economic losses. This research aimed to develop high-quality coffee mucilage capsules using spray drying technology. Chemically modified banana starch with octenyl succinic anhydride (OSA) and commercial maltodextrin were used as coating materials to enhance the properties of the capsules. Physicochemical and functional characterization was performed on samples of fresh and filtered coffee mucilage (MF), concentrated mucilage (MC), concentrated mucilage with the addition of maltodextrin and OSA-modified starch (MCMA), and finally, spray-dried coffee mucilage powder (MP). The antioxidant capacity (AC) of the mucilage was evaluated throughout the processing stages. MF showed an AC of 179.2 µmol of trolox/100 g, while the final coffee mucilage powder (MP) showed a significantly higher AC of 5444.35 µmol of trolox/100 g. Additionally, the MP showed a stability index of 0.48, water activity (aw) of 0.19, solubility of 14.64%, and a high water retention capacity of 90.53%. Microscopic analysis revealed amorphous structures with an average size of 29.16 ± 2.12 µm in the MP. These findings highlight the potential of spray drying with food-grade matrices such as OSA-modified banana starch to encapsulate coffee mucilage, preserving its antioxidant capacity and creating a new functional food ingredient with water retention properties.
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利用化学改性香蕉淀粉通过喷雾干燥获得咖啡粘液微胶囊
随着全球咖啡消费量的不断增长,哥伦比亚已成为全球第三大咖啡生产国。然而,咖啡豆在加工过程中会产生大量副产品,如富含抗氧化酚类化合物的粘液。这些废物处理不当会造成环境问题和经济损失。这项研究旨在利用喷雾干燥技术开发高质量的咖啡粘液胶囊。使用辛烯基丁二酸酐(OSA)化学改性香蕉淀粉和商品麦芽糊精作为包衣材料,以提高胶囊的性能。对新鲜和过滤咖啡粘液(MF)、浓缩粘液(MC)、添加麦芽糊精和 OSA 改性淀粉的浓缩粘液(MCMA)以及喷雾干燥咖啡粘液粉(MP)样品进行了理化和功能表征。在整个加工阶段都对粘液的抗氧化能力(AC)进行了评估。MF 的抗氧化能力为 179.2 µmol trolox/100g,而最终的咖啡粘液粉(MP)的抗氧化能力明显更高,达到 5444.35 µmol trolox/100g。显微分析显示,MP 中的无定形结构平均尺寸为 29.16 ± 2.12 µm。这些发现凸显了使用食品级基质(如 OSA 改性香蕉淀粉)进行喷雾干燥封装咖啡粘液的潜力,既能保持咖啡粘液的抗氧化能力,又能创造出一种具有保水特性的新型功能性食品配料。
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