Achieving balanced mechanical properties in laser powder bed fusion processed Inconel 718 superalloy through a simplified heat treatment process

IF 11.2 1区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY Journal of Materials Science & Technology Pub Date : 2024-08-28 DOI:10.1016/j.jmst.2024.06.057
Ziyi Ding, Kesong Miao, Qi Chao, Xinliang Xie, Xia Ji, Hao Wu, Xiaojun Wang, Guohua Fan
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Abstract

Laser additively manufactured (LAM) Ni-based superalloys commonly exhibit low strength and high residual stress in the as-built state, requiring post-heat treatment to improve mechanical properties. We propose a modified heat treatment (MHT) process that only involves a single-step aging at 650°C for 4 h to achieve high strength, high ductility, and low residual stress simultaneously in a laser powder bed fusion (LPBF)-processed Inconel 718 (IN718) alloy. The MHT treated alloy exhibits comparable tensile strength (1368 MPa) to the conventional solution plus two-step aging (SA) treated alloy (1398 MPa), while the tensile elongation (∼21.7% for MHT treated alloy and 13.4% for SA treated alloy) is 60% higher and the residual stress (∼195 MPa) is 20% lower than the SA treated alloy. The balanced high performance of the MHT IN718 alloy was mainly attributed to the precipitation of abundant γ" phase with a size of ∼5 nm, while the original nano-sized Laves precipitates and dislocation cells were mostly retained. The finer size and higher fraction of γ" of the MHT sample mainly result from the dislocation structure and compositional variations in the as-built IN718, which promotes precipitation during aging. The retention of Laves phase, and cellular dislocation network in the MHT alloy also contributes to work hardening during tension and suspends the occurrence of necking. This study unveils a unique strengthening and toughening mechanism in the Ni-based superalloy produced by LAM with the presence of abundant Laves precipitates and provides a simple, low energy-consumption and cost-effective heat treatment route for achieving desirable mechanical properties.

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通过简化热处理工艺实现激光粉末床熔融加工 Inconel 718 超级合金的均衡机械性能
激光快速成型(LAM)镍基超合金在成型状态下通常强度低、残余应力大,需要进行后热处理以改善机械性能。我们提出了一种改良热处理(MHT)工艺,只需在 650°C 下进行 4 小时的单步时效处理,即可在激光粉末床熔融(LPBF)加工的 Inconel 718 (IN718) 合金中同时实现高强度、高延展性和低残余应力。经 MHT 处理的合金的拉伸强度(1368 兆帕)与传统固溶加两步时效(SA)处理的合金(1398 兆帕)相当,而拉伸伸长率(MHT 处理的合金为 21.7%,SA 处理的合金为 13.4%)比 SA 处理的合金高 60%,残余应力(195 兆帕)比 SA 处理的合金低 20%。MHT IN718 合金的均衡高性能主要归功于析出了大量尺寸为 ∼5 nm 的 γ "相,而原有的纳米级 Laves 沉淀和位错晶胞大部分被保留了下来。MHT 样品的粒度更细,γ "的比例更高,这主要是由于坯料 IN718 中的位错结构和成分变化在老化过程中促进了析出。MHT 合金中保留的 Laves 相和蜂窝状位错网络也有助于拉伸过程中的加工硬化,并阻止了缩颈现象的发生。这项研究揭示了 LAM 法生产的镍基超合金中存在大量拉维斯析出物的独特强化和韧化机制,并为获得理想的机械性能提供了一种简单、低能耗且经济高效的热处理方法。
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来源期刊
Journal of Materials Science & Technology
Journal of Materials Science & Technology 工程技术-材料科学:综合
CiteScore
20.00
自引率
11.00%
发文量
995
审稿时长
13 days
期刊介绍: Journal of Materials Science & Technology strives to promote global collaboration in the field of materials science and technology. It primarily publishes original research papers, invited review articles, letters, research notes, and summaries of scientific achievements. The journal covers a wide range of materials science and technology topics, including metallic materials, inorganic nonmetallic materials, and composite materials.
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