Measuring depth-dependent residual stresses in gaseous nitrided steels using indentation method

IF 1.8 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Research Express Pub Date : 2024-08-29 DOI:10.1088/2053-1591/ad719c
Ahmet Fatih Yayla, Ridvan Gecu, Nuri Solak, Kursat Kazmanli, Mustafa Urgen
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Abstract

This study investigated residual stress evaluations during gaseous nitriding of 50CrMo4 and 31CrMoV9 steels. The nitriding processes were carried out in the NH3/H2/N2 atmosphere at 525 °C for 2 h by controlling the nitriding potential. The development of depth-dependent residual stresses was conducted using a Vickers indentation instrument with an estimated geometric correction. The obtained results correlated with the sublayer removal-assisted XRD sin2ψ method. Diffusion layers between 135 and 200 μm were obtained for all samples upon nitriding. The surface hardness values reached 475 HV for 50CrMo4 and 825 HV for 31CrMoV9 steels. The geometric correction factor α was calculated as 78° for a Vickers indenter to measure residual stresses. The generated compressive residual stresses by nitriding increased with increasing nitriding potential by 71% (from −350 to −600 MPa) and 13% (from −750 to −850 MPa) for 50CrMo4 and 31CrMoV9 steels, respectively. An approximately linear relationship was obtained between the hardness and residual stress profiles of the nitrided samples.
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利用压痕法测量气体氮化钢中随深度变化的残余应力
本研究调查了 50CrMo4 和 31CrMoV9 钢气体氮化过程中的残余应力评估。通过控制氮化电位,氮化过程在 525 °C 的 NH3/H2/N2 大气中进行了 2 小时。使用维氏压痕仪和估算的几何校正对深度相关残余应力进行了分析。获得的结果与次层去除辅助 XRD sin2ψ 方法相关。氮化后,所有样品都获得了 135 至 200 μm 的扩散层。50CrMo4 钢的表面硬度值达到 475 HV,31CrMoV9 钢的表面硬度值达到 825 HV。用维氏压头测量残余应力时,几何校正系数 α 的计算值为 78°。对于 50CrMo4 和 31CrMoV9 钢材,氮化产生的压缩残余应力随着氮化电位的增加分别增加了 71%(从 -350 到 -600 兆帕)和 13%(从 -750 到 -850 兆帕)。氮化样品的硬度和残余应力曲线之间存在近似线性关系。
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来源期刊
Materials Research Express
Materials Research Express MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
4.50
自引率
4.30%
发文量
640
审稿时长
12 weeks
期刊介绍: A broad, rapid peer-review journal publishing new experimental and theoretical research on the design, fabrication, properties and applications of all classes of materials.
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