In-Situ EBSD Study of Austenitisation in a Wire-Arc Additively Manufactured High-Strength Steel

M Taylor, Y H Mozumder, A D Smith, A E Davis, F Scenini, P B Prangnell, E J Pickering
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Abstract

As-built high-strength steel wire-arc additive manufactured (WAAM) components often contain coarse columnar prior austenite grain (PAG) structures. These microstructures can result in poor mechanical properties, hence post-build re-austenitisation treatments are of interest to improve microstructures. Here, the potential for engineering austenite refinement was investigated using high-temperature in-situ EBSD with high temporal resolution. It was found that 300M first austenitised with a memory effect, reforming the columnar PAG structures in both morphology and crystallographic orientation. This was observed to occur by the coalescence of acicular austenite and happened earlier in the depleted dendritic regions. On further heating, austenite underwent recrystallisation without the application of external deformation via a discontinuous mechanism, involving the bulging of the prior high angle boundaries. Recrystallisation twins were also seen to form and grow alongside regular recrystallised grains. The predominance of discontinuous recrystallisation meant that a coarse grain structure was still retained after austenitisation, owing to the influence of a grain ‘swapping’ effect.
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线弧加成型高强度钢奥氏体化的原位 EBSD 研究
线弧添加剂制造(WAAM)的高强度钢构件通常含有粗大的柱状先奥氏体晶粒(PAG)结构。这些微观结构会导致机械性能低下,因此制造后的再奥氏体化处理对改善微观结构很有意义。在此,我们使用具有高时间分辨率的高温原位 EBSD 研究了工程奥氏体细化的潜力。研究发现,300M 首次奥氏体化具有记忆效应,在形态和结晶取向上重新形成了柱状 PAG 结构。据观察,这是通过针状奥氏体的凝聚发生的,在贫化树枝状区域发生得更早。进一步加热时,奥氏体在没有外部变形的情况下通过不连续机制发生再结晶,包括先前的高角边界隆起。再结晶孪晶也会与规则再结晶晶粒一起形成和生长。不连续再结晶占主导地位意味着,由于晶粒 "交换 "效应的影响,粗晶粒结构在奥氏体化后仍得以保留。
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