Influence of print-chamber oxygen content on the microstructure and properties of 3D-printed 316L

Abstract

Samples of 316L stainless steel have been prepared using laser-powder bed fusion from the same batch of powder using different print-chamber oxygen levels, ranging from 50 ppm to 1500 ppm. The oxide particle density is found to increase with oxygen content, while the cell structure is invariant with oxygen level and the grain size shows a relatively sharp transition for measured oxygen levels of above 450 ppm. Based on the microstructural observations it is suggested that the increasing oxygen levels leads to a transition in the solidification pattern. Samples printed at the higher oxygen level show higher strength and lower mechanical anisotropy than samples with a coarser grains structure printed at lower oxygen levels. The main influence of the higher oxide particle content on thermal stability is on the kinetics of recrystallization during isothermal annealing at 1000 °C.