Application of a multivariate approach to the study of chemometric and sensory profiles of cookies fortified with brewers’ spent grain

Antonietta Baiano, Anna Fiore, Mariacinzia Rutigliano, Barbara la Gatta
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Abstract

This work was aimed to investigate the effects of three factors on cookie quality: brewers’ spent grain (BSG) composition [65% malted barley and 35% of unmalted durum (DA) or soft (RI), or emmer (EM) wheats]; geographical origin of the cereals used in brewing (Daunia or Salento); and percentages of BSG in cookie formulation (30 or 40%). A control made of 100% Manitoba flour was produced. Statistical analyses were performed to evaluate the effects of those factors (Analysis of Variance), the possibility to distinguish the various types of cookies (Principal Component Analysis), and the relationships among variables (Pearson Correlation Analysis).The single and interactive effects of the three factors were significant for almost all variables. Cookies with 40% EM spent grains showed the highest ash, dietary fibre, and total phenolic contents but cookies with 30% DA or RI spent grains received the highest overall quality scores due to the higher intensity of their fresh baked flavour and their lower hardness and fibrousness. Based on the nutritional and sensory characteristics, cookies fortified with RI and DA were the best to consume. Although few physicochemical differences can be attributed to geographical origin, a slightly higher overall sensory score was assigned to those produced with Salento cereals. Principal Component Analysis showed a clear separation between the control made of 100% Manitoba flour and the group of fortified cookies. Among the latter, the cookies produced with RI and DA spent grains were indistinguishable from each other due to their similar quality characteristics.

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应用多元方法研究添加了啤酒糟的饼干的化学计量学和感官特征
这项工作旨在研究以下三个因素对饼干质量的影响:酿酒师用过的谷物(BSG)成分[65%的发芽大麦和 35%的未发芽硬质小麦(DA)或软质小麦(RI)或埃默尔小麦(EM)];酿酒所用谷物的地理来源(道尼亚或萨兰托);以及饼干配方中 BSG 的百分比(30% 或 40%)。此外,还制作了由 100% 马尼托巴面粉制成的对照组。进行了统计分析,以评估这些因素的影响(方差分析)、区分不同类型饼干的可能性(主成分分析)以及变量之间的关系(皮尔逊相关分析)。含 40% EM 废谷物的饼干灰分、膳食纤维和总酚类含量最高,但含 30% DA 或 RI 废谷物的饼干总体质量得分最高,原因是其新鲜烘焙风味更浓,硬度和纤维度较低。从营养和感官特征来看,添加了 RI 和 DA 的饼干最适于食用。虽然几乎没有理化差异可归因于地理来源,但使用萨兰托谷物生产的饼干的总体感官评分略高。主成分分析表明,100% 马尼托巴面粉制成的对照组与强化饼干组之间存在明显差异。在后者中,用 RI 和 DA 废谷物生产的饼干因其相似的质量特性而无法区分。
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