Pressure-Assisted Electrothermal Explosion Synthesis of Titanium Nickelide

IF 0.9 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Inorganic Materials Pub Date : 2024-03-10 DOI:10.1134/S0020168523100011
Yu. V. Bogatov, A. V. Shcherbakov, V. A. Shcherbakov, D. Yu. Kovalev, A. E. Sychev
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Abstract

Titanium nickelide alloys have been prepared by pressure-assisted electrothermal explosion (ETE) synthesis. We have examined the effect of Joule heating power on ETE parameters and the physicomechanical properties of the synthesized alloys. The results demonstrate that raising the electrical voltage applied to the starting mixture leads to a decrease in ignition time and increase in the maximum ETE temperature. The ignition temperature was 350°C, independent of the Joule heating power. X-ray diffraction characterization showed that the major phase in the alloys was NiTi. According to uniaxial compression test results, the compressive strength of the alloys is 1980 MPa. Their microhardness HV is 6.4 ± 0.8 GPa. Instrumental indentation has been used to determine their hardness under load (HM = 9.4 GPa) and characteristics of their plastic and elastic deformation. The synthesized alloys have been shown to have high plasticity.

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压力辅助电热爆炸合成镍化钛
通过压力辅助电热爆炸(ETE)合成法制备了钛镍合金。我们研究了焦耳加热功率对 ETE 参数和合成合金物理机械性能的影响。结果表明,提高对起始混合物施加的电压会导致点火时间缩短和 ETE 最高温度升高。点火温度为 350°C,与焦耳加热功率无关。X 射线衍射表征显示,合金中的主要相为镍钛。根据单轴压缩测试结果,合金的抗压强度为 1980 兆帕。它们的显微硬度 HV 为 6.4 ± 0.8 GPa。利用仪器压痕法测定了合金在负荷下的硬度(HM = 9.4 GPa)及其塑性和弹性变形的特征。结果表明,合成合金具有很高的塑性。
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来源期刊
Inorganic Materials
Inorganic Materials 工程技术-材料科学:综合
CiteScore
1.40
自引率
25.00%
发文量
80
审稿时长
3-6 weeks
期刊介绍: Inorganic Materials is a journal that publishes reviews and original articles devoted to chemistry, physics, and applications of various inorganic materials including high-purity substances and materials. The journal discusses phase equilibria, including P–T–X diagrams, and the fundamentals of inorganic materials science, which determines preparatory conditions for compounds of various compositions with specified deviations from stoichiometry. Inorganic Materials is a multidisciplinary journal covering all classes of inorganic materials. The journal welcomes manuscripts from all countries in the English or Russian language.
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