Molecular flow model of gas transmission rate test device with auxiliary chamber for high barrier film

IF 3.8 2区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Vacuum Pub Date : 2024-11-23 DOI:10.1016/j.vacuum.2024.113861
Liu Xiaofeng, Hu Baofa, Zhuang Jiafu, Chu Ruobo, Su Zhicong, Xie Qinglai
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Abstract

The oxygen barrier test of plastic film is an important step in the sealing and preservation process of food and drugs, and the system leakage is pivotal factor of the test device that affecting the efficiency and accuracy. In order to reduce the impact of system leakage on the oxygen barrier detection of plastic film, a test device with an auxiliary seal on the outer layer is designed by using series dual sealing structure technology. Based on the molecular flow states hypothesis, according to the conservation of gas throughput and the invariance of flow resistance, a mathematical model and simulation platform for permeability test of flexible packaging materials with high barrier with outer auxiliary sealing chamber and forward leakage are established. By using Laplace transform method, the analytical solutions and corresponding characteristics of the pressure and leakage rate changes in the inner and outer sealing chamber are discussed, and the equivalent test time expression of the forward leakage test device is derived. The simulation and measured results show that the equivalent test time of the test device with the outer auxiliary sealing chamber is much longer than 24 h, and the test results of the pressure change of the inner sealing chamber are the same as the ideal leak-free system. Compared with the single sealing structure test device, the test error of the same high barrier film permeability test is negligible. By using the test device with an auxiliary sealing chamber, the oxygen barrier property can be accurately measured without any leak measurement and correction.
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高阻隔膜辅助室气体透过率测试装置的分子流模型
塑料薄膜氧阻隔试验是食品、药品密封保鲜过程中的重要环节,而系统泄漏是影响试验装置效率和准确性的关键因素。为了减少系统泄漏对塑料薄膜氧障检测的影响,采用串联双密封结构技术,设计了一种外层有辅助密封的测试装置。基于分子流态假设,根据气体通量守恒和流动阻力不变性,建立了具有外辅助密封室和正向泄漏的高阻隔软包装材料渗透性测试的数学模型和仿真平台。利用拉普拉斯变换方法,讨论了内外密封腔内压力和泄漏率变化的解析解及相应特征,推导了正向泄漏试验装置的等效试验时间表达式。仿真和实测结果表明,外辅助密封室试验装置的等效试验时间远长于24 h,内密封室压力变化的试验结果与理想的无泄漏系统相同。与单一密封结构试验装置相比,相同高阻隔膜透气性试验的试验误差可以忽略不计。采用带辅助密封室的测试装置,可准确测量氧阻隔性能,无需进行泄漏测量和校正。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Vacuum
Vacuum 工程技术-材料科学:综合
CiteScore
6.80
自引率
17.50%
发文量
0
审稿时长
34 days
期刊介绍: Vacuum is an international rapid publications journal with a focus on short communication. All papers are peer-reviewed, with the review process for short communication geared towards very fast turnaround times. The journal also published full research papers, thematic issues and selected papers from leading conferences. A report in Vacuum should represent a major advance in an area that involves a controlled environment at pressures of one atmosphere or below. The scope of the journal includes: 1. Vacuum; original developments in vacuum pumping and instrumentation, vacuum measurement, vacuum gas dynamics, gas-surface interactions, surface treatment for UHV applications and low outgassing, vacuum melting, sintering, and vacuum metrology. Technology and solutions for large-scale facilities (e.g., particle accelerators and fusion devices). New instrumentation ( e.g., detectors and electron microscopes). 2. Plasma science; advances in PVD, CVD, plasma-assisted CVD, ion sources, deposition processes and analysis. 3. Surface science; surface engineering, surface chemistry, surface analysis, crystal growth, ion-surface interactions and etching, nanometer-scale processing, surface modification. 4. Materials science; novel functional or structural materials. Metals, ceramics, and polymers. Experiments, simulations, and modelling for understanding structure-property relationships. Thin films and coatings. Nanostructures and ion implantation.
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