Study on pilot-scale inline jet flow high shear mixer: Discharge, macro-mixing time, and residence time distribution

IF 13.2 1区 工程技术 Q1 ENGINEERING, CHEMICAL Chemical Engineering Journal Pub Date : 2024-12-26 DOI:10.1016/j.cej.2024.158812
Junbo Wu, Junheng Guo, Yudong Liu, Kangkang Ma, Yingcheng Wang, Wei Li, You Han, Ruan Chi, Bingwen Long, Jinli Zhang
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Abstract

High shear mixers with long residence times are essential to intensify finite rate reactions. Therefore, the discharge, residence time distribution (RTD), and macro-mixing time characteristics of a pilot-scale inline jet flow high shear mixer (JFHSM) were systematically investigated. Using experimental and CFD simulation methods, the effects of rotational speed N, feed flow rate QI, feed position, stator bottom opening ratio φ, and rotor angle α were studied. The results show that the inline JFHSM is a perfect mixing reactor, and the effect of QI is weak. The stator’s presence or increased N enhance dispersion and mixing effects. A closer feed position to the mixing head results in better dispersion and a smaller tM. Alterations to the φ and the α result in notable modifications to the flow pattern. tM is smaller at φ ≥ 0.250, with an optimal value at φ = 0.567, and the inline JFHSM has the smallest Po at α = 30° and the lowest tM at α = 90°.Moreover, the correlation equations for FlT, Po, Srave, A, and εave, A provide guidance for optimizing and scaling up inline JFHSM.
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中试规模直列射流高剪切混合器的研究:流量、宏观混合时间和停留时间分布
具有长停留时间的高剪切混合器对于加强有限速率反应是必不可少的。为此,对中试规模直列射流高剪切混合器(JFHSM)的流量、停留时间分布(RTD)和宏观混合时间特性进行了系统研究。采用实验和CFD模拟方法,研究了转速N、进给流量QI、进给位置、定子底开度比φ、转子角α等参数对转子转速的影响。结果表明,直列式JFHSM是一种理想的混合反应器,QI的影响较弱。定子的存在或N的增加增强了分散和混合效应。靠近混合头的进料位置可以得到更好的分散和更小的tM。φ和α的改变会导致流型的显著变化。在φ≥0.250时tM较小,φ = 0.567时tM最优,直列式JFHSM在α = 30°时Po最小,在α = 90°时tM最小。此外,FlT、Po、save、A和εave、A的相关方程为直线JFHSM的优化和放大提供了指导。
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来源期刊
Chemical Engineering Journal
Chemical Engineering Journal 工程技术-工程:化工
CiteScore
21.70
自引率
9.30%
发文量
6781
审稿时长
2.4 months
期刊介绍: The Chemical Engineering Journal is an international research journal that invites contributions of original and novel fundamental research. It aims to provide an international platform for presenting original fundamental research, interpretative reviews, and discussions on new developments in chemical engineering. The journal welcomes papers that describe novel theory and its practical application, as well as those that demonstrate the transfer of techniques from other disciplines. It also welcomes reports on carefully conducted experimental work that is soundly interpreted. The main focus of the journal is on original and rigorous research results that have broad significance. The Catalysis section within the Chemical Engineering Journal focuses specifically on Experimental and Theoretical studies in the fields of heterogeneous catalysis, molecular catalysis, and biocatalysis. These studies have industrial impact on various sectors such as chemicals, energy, materials, foods, healthcare, and environmental protection.
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