Investigation on the surface topography and surface/subsurface damage mechanisms of polycrystalline yttrium aluminum garnet ceramics in ultra-precision grinding

IF 5.5 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2025-02-01 Epub Date: 2024-12-25 DOI:10.1016/j.matchar.2024.114688
Hang Yin, Sheng Wang, Qingliang Zhao
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Abstract

This study investigates the surface topography and surface/subsurface damage mechanisms of polycrystalline yttrium aluminum garnet (YAG) ceramics in ultra-precision grinding. Firstly, the impacts of grinding parameters on the depth of subsurface damage was studied using the cross-sectional polishing method. Secondly, focused ion beam (FIB) thinning and transmission electron microscopy (TEM) were applied to observe the subsurface damage of YAG ceramics in ultra-precision grinding. Finally, the effect of process arguments on the formation of subsurface damage of polycrystalline YAG ceramics in ultra-precision grinding was analyzed. The results indicate that process parameters significantly affect the surface/subsurface damage defects of YAG ceramics during ultra-precision grinding. The degree of effect follows the order: grinding depth (ap) > feed rate (F) > diamond wheel speed (ns) > workpiece speed (nw). The surface roughness increases with the increase of workpiece speed, feed speed and grinding depth, but the increase of grinding depth will lead to a steep increase in surface roughness, and the surface roughness under different parameters is positively correlated with the surface defects. The all-plastic ultra-precision grinding surface of YAG ceramics with a roughness of 6 nm can be achieved with the resin bonded D7 diamond grinding wheel under the process parameters of the grinding speed is 7000 rpm, the workpiece speed is 60 rpm, the grinding depth is 0.5 μm, and the feed speed is 1.5 mm/min. The subsurface damage depth of YAG ultra-precision grinding is less affected by workpiece speed, and increases linearly with the increase of feed speed and wheel speed, and increases sharply with the increase of grinding depth. The transition from crystal to amorphous occurs in the grain, including atomic scale defects such as dislocation, layer fault and lattice distortion, which is the fundamental cause of subsurface microscopic damage.
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多晶钇铝石榴石陶瓷超精密磨削表面形貌及表面/亚表面损伤机理研究
研究了多晶钇铝石榴石(YAG)陶瓷在超精密磨削过程中的表面形貌和表面/亚表面损伤机理。首先,采用截面抛光法研究了磨削参数对亚表面损伤深度的影响。其次,利用聚焦离子束(FIB)细化和透射电镜(TEM)观察了YAG陶瓷在超精密磨削过程中的亚表面损伤。最后,分析了工艺参数对多晶YAG陶瓷超精密磨削亚表面损伤形成的影响。结果表明,工艺参数对YAG陶瓷超精密磨削过程中的表面/亚表面损伤缺陷有显著影响。影响程度依次为:磨削深度(ap) >;进给量(F) >;金刚石砂轮转速(ns) >;工件速度(nw)。表面粗糙度随工件速度、进给速度和磨削深度的增加而增加,但磨削深度的增加会导致表面粗糙度急剧增加,不同参数下的表面粗糙度与表面缺陷呈正相关。采用树脂结合剂D7金刚石砂轮,在磨削速度为7000 rpm、工件速度为60 rpm、磨削深度为0.5 μm、进给速度为1.5 mm/min的工艺参数下,可实现YAG陶瓷的粗糙度为6 nm的全塑料超精密磨削表面。YAG超精密磨削亚表面损伤深度受工件速度的影响较小,随进给速度和砂轮速度的增加而线性增加,随磨削深度的增加而急剧增加。晶粒从晶态到非晶态的转变发生在晶粒内部,包括位错、层错、晶格畸变等原子尺度缺陷,这是造成亚表面微观损伤的根本原因。
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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