Evaluating neon ions as an alternative to gallium in micro cantilevers fracture testing

IF 5.6 2区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Scripta Materialia Pub Date : 2025-03-15 Epub Date: 2024-12-16 DOI:10.1016/j.scriptamat.2024.116509
Eloho Okotete , Stefan Mück , Subin Lee , Christoph Kirchlechner
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Abstract

The influence of neon ions at the notch front as well as of annealing heat treatments on the fracture toughness of single crystalline silicon was investigated via microcantilever fracture testing. Using in situ scanning electron microscope deformation, the fracture toughness of the neon-notched cantilevers after annealing was measured, resulting in an average value of 1.0 MPa m0.5, proving that chemically inert gas ions can result in similar fracture toughness values as with Ga FIBs. However, Ne bubble formation was identified as substantial source of errors and we advise caution when interpreting fracture toughness measurements when using Ne as chemically inert ion species for notching.

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评价氖离子在微悬臂断裂测试中作为镓的替代品
通过微悬臂断裂试验研究了缺口前缘氖离子和退火热处理对单晶硅断裂韧性的影响。采用原位扫描电镜变形法测量了氖缺口悬臂梁退火后的断裂韧性,其平均值为1.0 MPa m0.5,证明化学惰性气体离子可以产生与Ga FIBs相似的断裂韧性值。然而,Ne气泡的形成被认为是误差的主要来源,我们建议在使用Ne作为化学惰性离子进行缺口时解释断裂韧性测量时要谨慎。
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来源期刊
Scripta Materialia
Scripta Materialia 工程技术-材料科学:综合
CiteScore
11.40
自引率
5.00%
发文量
581
审稿时长
34 days
期刊介绍: Scripta Materialia is a LETTERS journal of Acta Materialia, providing a forum for the rapid publication of short communications on the relationship between the structure and the properties of inorganic materials. The emphasis is on originality rather than incremental research. Short reports on the development of materials with novel or substantially improved properties are also welcomed. Emphasis is on either the functional or mechanical behavior of metals, ceramics and semiconductors at all length scales.
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