Effect of the scanning strategy on texture of grain-oriented electrical steel (Fe-4wt%Si) processed via laser powder-bed fusion and subsequent thermomechanical processing

IF 5.5 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2025-01-28 DOI:10.1016/j.matchar.2025.114789
M.S. Lyrio , H.R. Oliveira , M.J.R. Sandim , V. Devulapalli , H.R.Z. Sandim
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Abstract

Abnormal grain growth is a fundamental phenomenon in the processing of grain-oriented electrical steels. The presence of inhibitors, strong texture, and reduced sheet thickness are key factors that contribute to its occurrence. In this work, a grain-oriented electrical steel (Fe-4wt%Si) was obtained using laser powder bed fusion (LPBF) additive manufacturing and subsequent thermomechanical processing. The LPBF-processed slabs were built using scanning strategies without rotation (0°) and with rotations of 45° and 90° between the layers. Subsequently, the slabs were cold rolled to 91 % reduction. Abnormal grain growth occurred during prolonged box annealing at 1200 °C, favored by the coarsening of crystalline SiO2-based nanoparticles that acted as inhibitors of normal grain growth. The influence of the scanning strategy on the as-built texture and the magnetic properties after thermomechanical processing was investigated. Very coarse grain sizes, low porosity and reduced thickness contributed positively to the decrease in magnetic losses. The deviation of Goss grains from the ideal orientation was smaller for samples without rotation (0o), indicating that this scanning strategy generates textures closer to the desired ones (Goss and η fiber). This strategy provided the lowest magnetic losses and the best magnetic properties among the laser scanning strategies investigated.

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扫描策略对激光粉末床熔合及后续热处理晶粒取向电工钢(Fe-4wt%Si)织构的影响
晶粒生长异常是晶粒取向电工钢加工过程中的一个基本现象。抑制剂的存在、强织构和薄板厚度的减小是导致其发生的关键因素。在这项工作中,采用激光粉末床熔合(LPBF)增材制造和随后的热机械加工获得了晶粒取向电工钢(Fe-4wt%Si)。采用无旋转(0°)和层间旋转45°和90°的扫描策略构建lpbf加工板。随后,对板坯进行冷轧,降低到91%。在1200℃的长时间箱形退火过程中,晶粒出现了异常生长,这是由于晶体sio2基纳米颗粒的粗化,起到了抑制正常晶粒生长的作用。研究了热处理后扫描策略对成形织构和磁性能的影响。非常粗的晶粒尺寸、低孔隙率和厚度的减小对磁损耗的降低有积极的贡献。在没有旋转(0)的情况下,Goss晶粒与理想取向的偏差较小,这表明这种扫描策略产生的织构更接近于期望的织构(Goss和η纤维)。在所研究的激光扫描策略中,该策略具有最低的磁损耗和最佳的磁性能。
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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