Introducing mechanism of nano planar defect structure in Ti-48Al-2Nb-2Cr alloy through muti-step heat treatment and its effect on mechanical properties

IF 5.5 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Materials Characterization Pub Date : 2025-04-01 Epub Date: 2025-02-05 DOI:10.1016/j.matchar.2025.114820
Qing Hu , Yan Wang , Yong Liu , Liang Su , Jingjun He , Yaofeng Luo , Hanghao Gao , Bin Liu , Liangxing Lv
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Abstract

Improving the comprehensive properties of γ-TiAl alloys is of important engineering significance, and nano planar defect structure (NPDS), including stacking faults (SFs) and nano twins, etc. have shown a great strengthening effect in many alloys. In this paper, a relatively simple and feasible multi-step heat treatment method was adopted to introduce NPDS into an as-forged Ti-48Al-2Nb-2Cr alloy. The repeated phase transformation in cyclic heat treatment (CHT) resulted in the formation of NPDS in equiaxed grains, which was closely related to the phase transformation of α(α2) → FCC → γ. The morphology of NPDS was associated with the formation rate of FCC regions. With the increase of cycle times, complex twin boundaries and SF regions were formed. After short heat treatment (SHT) and aging, the NPDS reinforced alloy with duplex phase (DP) structure was finally obtained, which exhibited similar grain size with the as-forged alloy. The tensile strength of the heat-treated alloy at room temperature and 700 °C reached 839 MPa and 714 MPa. The significant advantage in tensile strength can be attributed to the obvious inhibition of NPDS on dislocation slip. The formation of the interface dislocation loops as well as the wide distributions of pseudo twin (PT) and rotational boundary (RB) played a beneficial role in improving the plasticity and fracture toughness of the alloy.
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介绍了Ti-48Al-2Nb-2Cr合金多步热处理后纳米平面缺陷组织形成机理及其对力学性能的影响
提高γ-TiAl合金的综合性能具有重要的工程意义,纳米平面缺陷结构(NPDS),包括层错(SFs)和纳米孪晶等在许多合金中都表现出了很强的强化作用。本文采用一种相对简单可行的多步热处理方法,将NPDS引入锻造态Ti-48Al-2Nb-2Cr合金中。循环热处理(CHT)的反复相变导致等轴晶中NPDS的形成,这与α(α2)→FCC→γ的相变密切相关。NPDS的形态与FCC区的形成速率有关。随着循环次数的增加,形成了复杂的孪晶界和SF区。经过短时间热处理(SHT)和时效处理,最终获得了具有双相组织(DP)的NPDS增强合金,其晶粒尺寸与锻造态合金相似。热处理后的合金在室温和700℃的抗拉强度分别达到839 MPa和714 MPa。NPDS在抗拉强度上的显著优势可归因于其对位错滑移的明显抑制作用。界面位错环的形成以及伪孪晶(PT)和旋转边界(RB)的广泛分布有利于提高合金的塑性和断裂韧性。
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来源期刊
Materials Characterization
Materials Characterization 工程技术-材料科学:表征与测试
CiteScore
7.60
自引率
8.50%
发文量
746
审稿时长
36 days
期刊介绍: Materials Characterization features original articles and state-of-the-art reviews on theoretical and practical aspects of the structure and behaviour of materials. The Journal focuses on all characterization techniques, including all forms of microscopy (light, electron, acoustic, etc.,) and analysis (especially microanalysis and surface analytical techniques). Developments in both this wide range of techniques and their application to the quantification of the microstructure of materials are essential facets of the Journal. The Journal provides the Materials Scientist/Engineer with up-to-date information on many types of materials with an underlying theme of explaining the behavior of materials using novel approaches. Materials covered by the journal include: Metals & Alloys Ceramics Nanomaterials Biomedical materials Optical materials Composites Natural Materials.
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