Zinc vanadate nanoparticle: An innovative electrochemical sensor synthesized via green fuel for the detection of ascorbic acid and its other applications

IF 3.4 4区 化学 Q2 CHEMISTRY, MULTIDISCIPLINARY Journal of the Indian Chemical Society Pub Date : 2025-03-01 Epub Date: 2025-02-03 DOI:10.1016/j.jics.2025.101607
H. Anantharama , J.R. Naveen Kumar , M. Rohit , Divya R. Basavannavar , B.M. Praveen , Asad Syed , R. Harini , G. Nagaraju , Bharath K. Devendra
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Abstract

Zinc vanadate (Zn4V2O9) nanoparticles (NPs) have been effectively produced at 600 °C using the solution combustion technique. The as-synthesized Zn4V2O9 NPs were further examined using a variety of methods, including photoluminescence (PL), Fourier transform infrared spectroscopy (FTIR), ultraviolet–visible spectroscopy (UV–Vis), and X-ray diffraction (XRD), to look at the surface morphological characteristics of a material or sample as well as its optical and crystal structural characteristics. Additionally, the synthesized Nps is employed in various processes including photocatalytic dye degradation of Rose Bengal dye and latent finger printing.Zn4V2O9 NPs were discovered to have a crystal size of 45.97 nm, and the XRD pattern indicates that the synthesized NPs had a monoclinic crystallite structure. Scanning electron microscopy (SEM) is used to identify the shape of NPs. l-Ascorbic acid (LAA) presence is detected using the produced NPs. This study involves dropcasting of NPs and electrode modification. The electrode is utilized for additional research after being left overnight to dry.

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钒酸锌纳米颗粒:利用绿色燃料合成的一种新型电化学传感器,用于检测抗坏血酸及其其他应用
采用溶液燃烧技术,在600℃下制备了钒酸锌纳米颗粒(Zn4V2O9)。利用光致发光(PL)、傅里叶变换红外光谱(FTIR)、紫外可见光谱(UV-Vis)和x射线衍射(XRD)等多种方法对合成的Zn4V2O9 NPs进行了进一步的检测,以观察材料或样品的表面形态特征以及光学和晶体结构特征。此外,合成的Nps还被用于光催化降解玫瑰染料和潜在指纹等多种工艺。Zn4V2O9 NPs的晶粒尺寸为45.97 nm, XRD谱图表明合成的NPs具有单斜晶结构。扫描电子显微镜(SEM)用于鉴定NPs的形状。利用生成的NPs检测l-抗坏血酸(LAA)的存在。本研究涉及NPs的投射和电极修饰。电极在过夜干燥后用于额外的研究。
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来源期刊
CiteScore
3.50
自引率
7.70%
发文量
492
审稿时长
3-8 weeks
期刊介绍: The Journal of the Indian Chemical Society publishes original, fundamental, theorical, experimental research work of highest quality in all areas of chemistry, biochemistry, medicinal chemistry, electrochemistry, agrochemistry, chemical engineering and technology, food chemistry, environmental chemistry, etc.
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