Structure-activity relationship on tensile properties under DRX and slip system activity of U-CVCDEed AZ31 magnesium alloy

IF 13.8 1区 材料科学 Q1 METALLURGY & METALLURGICAL ENGINEERING Journal of Magnesium and Alloys Pub Date : 2025-08-01 Epub Date: 2025-04-02 DOI:10.1016/j.jma.2025.03.010
Qiang Liu , Feng Li , Fu Wei Kang , Hai Bo Wang , Shun Luo
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Abstract

Given the limitations of traditional hot extrusion methods in improving the microstructure and mechanical properties of magnesium(Mg) alloys, this paper attempts to treat AZ31 Mg alloy billet by pre-upsetting continuous variable cross-section direct extrusion (U-CVCDE). The effects of dynamic recrystallization behavior and slip system activity on texture evolution and mechanical properties of CVCDE Mg alloys with different pre-upsetting amounts were systematically analyzed. The results indicate that the introduction of the pre-upsetting process promotes dynamic recrystallization during the CVCDE process. The recrystallization proportion shows a trend of first rising and then decreasing with the increase of the pre-upsetting amount. Among them, the proportion of recrystallization grains in the U2-CVCDE-formed structural parts is as high as 88.3%. The average grain sizes of U1-CVCDE, U2-CVCDE, and U3-CVCDE were 6.01 µm, 4.90 µm, and 10.45 µm, respectively. In addition, following U-CVCDE, the pyramidal slip of each forming component consistently maintains a high level of activation and opening and dominates, making more grains deflect in the axial extrusion direction of C to varying degrees, which is conducive to the uniform distribution of stress in more grains during plastic deformation. The synergistic effect of dynamic recrystallization behavior and the high activity of the pyramidal slip system significantly weakened the (0001) basal texture strength, and the maximum basal texture strength showed a gradually decreasing trend, among which the base surface texture strength of U3-CVCDE formed parts was only 9.9. The U-CVCDE process is employed to achieve deep modification of Mg alloy, and excellent comprehensive mechanical properties are obtained; among them, the yield and tensile strength of U2-CVCDE are as high as 243.4 MPa and 317.5 MPa, respectively, and the elongation after breaking is up to 21.3%. This study introduces a practical new idea for investigating the extrusion forming technology of high-performance Mg alloys.

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AZ31镁合金在DRX作用下拉伸性能及滑移体系活性的构效关系
针对传统热挤压方法在改善镁合金组织和力学性能方面的局限性,采用预镦粗连续变截面直接挤压法(U-CVCDE)对AZ31镁合金坯料进行了处理。系统分析了动态再结晶行为和滑移系统活性对不同预镦粗量CVCDE镁合金织构演变和力学性能的影响。结果表明,预镦粗工艺的引入促进了CVCDE过程的动态再结晶。随着预镦粗量的增加,再结晶率呈现先升高后降低的趋势。其中,在u_2 - cvcde形成的结构件中,再结晶晶粒所占比例高达88.3%。U1-CVCDE、U2-CVCDE和U3-CVCDE的平均晶粒尺寸分别为6.01µm、4.90µm和10.45µm。此外,在U-CVCDE过程中,各成形构件的锥体滑移始终保持较高的激活度和开度并占主导地位,使得更多的晶粒不同程度地向C轴向挤压方向偏转,有利于塑性变形过程中应力在更多的晶粒中均匀分布。动态再结晶行为和高活性锥体滑移体系的协同作用显著削弱了(0001)基面织构强度,最大基面织构强度呈逐渐降低的趋势,其中U3-CVCDE成形件基面织构强度仅为9.9。采用U-CVCDE工艺对镁合金进行深度改性,获得了优异的综合力学性能;其中,U2-CVCDE的屈服强度和抗拉强度分别高达243.4 MPa和317.5 MPa,断裂伸长率高达21.3%。本研究为高性能镁合金挤压成形技术的研究提供了一种实用的新思路。
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来源期刊
Journal of Magnesium and Alloys
Journal of Magnesium and Alloys Engineering-Mechanics of Materials
CiteScore
20.20
自引率
14.80%
发文量
52
审稿时长
59 days
期刊介绍: The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.
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