Unveiling anomalous strengthening and deformation mechanism evolution in a Mg-Gd-Y-Zr alloy under rate-temperature coupling effects

IF 13.8 1区 材料科学 Q1 METALLURGY & METALLURGICAL ENGINEERING Journal of Magnesium and Alloys Pub Date : 2025-06-01 Epub Date: 2025-04-15 DOI:10.1016/j.jma.2025.03.018
Jingli Li , Chen Wen , Xiuzhu Han
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Abstract

While the deformation behavior of rare-earth magnesium alloys at high temperatures has been extensively studied, the deformation mechanisms under moderate-to-low temperatures and high strain rates remain insufficiently understood. To address this gap, hot compression tests were conducted on a Mg-11Gd-3Y-0.5Zr (wt.%) alloy over a temperature range of 150 °C–450 °C under strain rates of 10⁻³ s⁻¹ (low strain rate (LSR)) and 10 s⁻¹ (high strain rate (HSR)) to explore the strain rate-temperature coupling effects during hot deformation. The results revealed an anomalous increase in peak stress at 150 °C–250 °C as the strain rate decreased, attributed to the combined effects of nano-precipitates, dislocation cell structures, and serrated flow induced by dynamic strain aging. At higher temperatures, strain rate influences softening pathways: under HSR at 450 °C, the effect of twinning shifts from strengthening to facilitating dynamic recrystallization (DRX), resulting in substantial grain refinement (∼4 µm, 81% area fraction at a strain of 0.6). In contrast, at LSR, softening is dominated by dynamic recovery at 350 °C, with limited DRX (∼4 µm grains, 10% area fraction at a strain of 0.6) occurs at 400 °C. These findings clarify the dual role of twinning and its interaction with rate-temperature conditions, providing valuable insights into optimizing the hot processing of rare-earth magnesium alloys.

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揭示速率-温度耦合作用下Mg-Gd-Y-Zr合金的异常强化和变形机制演变
虽然稀土镁合金在高温下的变形行为已经得到了广泛的研究,但对中低温和高应变速率下的变形机制仍然知之甚少。为了解决这一差距,对Mg-11Gd-3Y-0.5Zr (wt.%)合金在150°C - 450°C的温度范围内进行热压缩试验,在10⁻³⁻¹(低应变速率(LSR))和10 s⁻¹(高应变速率(HSR))的应变速率下进行热变形,以探索热变形过程中的应变速率-温度耦合效应。结果表明,在150°C - 250°C时,随着应变速率的降低,峰值应力出现了反常的增加,这是由于纳米析出物、位错细胞结构和动态应变时效引起的锯齿状流动的共同作用。在更高的温度下,应变速率影响软化路径:在450°C的HSR下,孪晶的作用从强化转变为促进动态再结晶(DRX),导致大量晶粒细化(~ 4µm,面积分数为81%,应变为0.6)。相比之下,在LSR下,软化主要是在350°C时的动态恢复,在400°C时发生有限的DRX(~ 4µm晶粒,在0.6应变下面积分数为10%)。这些发现阐明了孪晶的双重作用及其与速率-温度条件的相互作用,为优化稀土镁合金的热加工提供了有价值的见解。
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来源期刊
Journal of Magnesium and Alloys
Journal of Magnesium and Alloys Engineering-Mechanics of Materials
CiteScore
20.20
自引率
14.80%
发文量
52
审稿时长
59 days
期刊介绍: The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.
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