Clarifying interfacial microstructures of Ti particle reinforced Mg-Zn-Mn composites to achieve good strength-ductility synergy

IF 13.8 1区 材料科学 Q1 METALLURGY & METALLURGICAL ENGINEERING Journal of Magnesium and Alloys Pub Date : 2025-12-01 Epub Date: 2025-04-26 DOI:10.1016/j.jma.2025.03.030
Jichuan Fan , Hong Yang , Wenlong Xie , Gong Chen , Yunxuan Zhou , Kaihong Zheng , Jun Xu , Jun Tan , Xianhua Chen , Fusheng Pan
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Abstract

In the field of particle reinforced magnesium (Mg) matrix composites (MMCs), the interfacial microstructures between reinforcements and Mg matrix are a subject of interest for most researchers. In this work, the 2 wt.% Ti particle reinforced Mg-6Zn alloy composites with different contents (0, 0.5, 1, 1.5, 2 wt.%) of Mn were prepared using semi-solid stirring assisted ultrasonic treatment followed by hot extrusion. With the increment of Mn element, the characteristics of mixed-grain structure became obvious and the DRX was inhibited. Meanwhile, the interfacial product gradually changed from MgZn2 to Mn2Ti. The tensile test demonstrated that the 2Ti/Mg-6Zn-1.5Mn composite exhibited an excellent strength-ductility synergy, achieving the highest yield stress (YS), ultimate tensile stress (UTS) of 239 MPa, 366 MPa, respectively, along with a notable elongation (El.) of 20.6%. The increased strength is mainly due to the grain refinement, the precipitation strengthening, the HDI strengthening and the strong interfacial bonding including the tightly Ti/Mn2Ti bonding and the Mn2Ti/Mg coherent orientation relationship. The ideal El. is the result of fine/coarse bimodal structure and the proper interfacial reaction, which can reduce the occurrence of cracks.

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澄清Ti颗粒增强Mg-Zn-Mn复合材料的界面微观结构,实现良好的强度-延性协同
在颗粒增强镁基复合材料(MMCs)中,增强材料与镁基之间的界面微观结构一直是研究人员感兴趣的课题。采用半固体搅拌辅助超声处理和热挤压法制备了Mn含量分别为0、0.5、1、1.5、2 wt.%的2 wt.% Ti颗粒增强Mg-6 Zn合金复合材料。随着Mn元素的增加,混合晶粒结构的特征变得明显,DRX受到抑制。同时,界面产物由MgZn2逐渐转变为Mn2Ti。拉伸试验表明,2Ti/Mg-6Zn-1.5Mn复合材料具有良好的强度-塑性协同效应,最高屈服应力(YS)为239 MPa,极限拉伸应力(UTS)为366 MPa,延伸率(El)为20.6%。强度的提高主要是由于晶粒细化、析出强化、HDI强化和强界面结合,包括紧密的Ti/Mn2Ti结合和Mn2Ti/Mg共格取向关系。理想的El。是细/粗双峰结构和适当的界面反应的结果,这可以减少裂纹的发生。
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来源期刊
Journal of Magnesium and Alloys
Journal of Magnesium and Alloys Engineering-Mechanics of Materials
CiteScore
20.20
自引率
14.80%
发文量
52
审稿时长
59 days
期刊介绍: The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.
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