Incorporation of Treated Woven Carbon Fiber to Methacrylate Resin for Heat-Cured Acrylic Denture Composite

IF 0.5 Q4 ENGINEERING, BIOMEDICAL Journal of Biomimetics, Biomaterials and Biomedical Engineering Pub Date : 2022-05-20 DOI:10.4028/p-627g18
Wafaa A. Hussain, M. Ismail, S. Taher
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引用次数: 2

Abstract

This research has studied the addition effect of woven carbon fiber treated with NaOH and coated by β- TCP to the conventional polymethyl methacrylate (PMMA). Two stages are involved in the preparation of heat-cured acrylic denture composite. The first chemical treatment of woven carbon fiber (WCF) surface by different concentrations of NaOH (0.10, 0.15, and 0.20 M) and coating carbon fiber with β-TCP by various weight fractions (0.08, 0.10, and 0.12 wi) were carried out. The second stage includes the reinforcement of denture base material by treated and coated WCF. The functional groups of the WCF surface before and after alkali treatment were studied by FTIR. The morphology of the WCF surface before and after alkali treatment was observed by FESEM, the diameter of pores on the untreated and treated fibers, and the adhesion of β-TCP powder to the fiber was also observed. Mechanical tests include: impact strength (I.S.) and flexural strength (F.S) were calculated using a three-point bending test with a universal test machine and a Charpy impact test machine, respectively. From the result, reinforcing PMMA with treated and coated WCF improves the mechanical properties (impact and flexural strength).
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经处理的编织碳纤维掺入甲基丙烯酸树脂热固化丙烯酸义齿复合材料
研究了经NaOH处理后β- TCP包覆的编织物碳纤维对常规聚甲基丙烯酸甲酯(PMMA)的添加效果。热固化丙烯酸义齿复合材料的制备涉及两个阶段。首先用不同浓度的NaOH(0.10、0.15和0.20 M)对编织碳纤维(WCF)表面进行化学处理,然后用不同质量分数(0.08、0.10和0.12 wi)的β-TCP涂覆碳纤维。第二阶段包括处理和涂层的WCF对义齿基托材料的加固。用红外光谱研究了碱处理前后WCF表面的官能团。用FESEM观察碱处理前后WCF的表面形貌、未处理和处理纤维的孔直径以及β-TCP粉末对纤维的粘附性。力学试验包括:冲击强度(I.S.)和抗弯强度(f.s.)分别采用通用试验机和夏比冲击试验机进行三点弯曲试验计算。从结果来看,用处理和涂层的WCF增强PMMA可以改善机械性能(冲击和弯曲强度)。
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CiteScore
1.40
自引率
14.30%
发文量
73
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