Synthesis, Characterization, and Dye Removal Applications of Graphene Oxide-Gold Nanocomposite

Q3 Biochemistry, Genetics and Molecular Biology Biointerface Research in Applied Chemistry Pub Date : 2022-10-31 DOI:10.33263/briac134.385
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Abstract

Here, we report the facile synthesis of graphene oxide/gold nanocomposite, and dye removal ability as an adsorbent was studied. Sodium citrate as a reducing agent was used to reduce Au (III) ions to the formation of gold nanoparticles on the surface of graphene oxide sheets that were prepared by Hummers’ method. Transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR), and X-ray diffraction (XRD) was used to specify nanocomposite synthesis. Adsorption dosage and contact time were investigated and explained as influencing parameters in removing methylene blue and methyl orange. In optimum conditions, the amount of adsorbent 30 mg and contact time 15 min for methylene blue and the amount of adsorbent 30 mg and contact time 25 min for methyl orange were quantitatively removed from 10 mL of wastewater. The pseudo-second-order model explained the kinetic data. Since graphene oxide/gold nanocomposite could be reused reasonably and had adsorptive properties, it tends to be produced as a modest and elective adsorbent to treat wastewater.
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氧化石墨烯-金纳米复合材料的合成、表征及除染应用
在这里,我们报道了氧化石墨烯/金纳米复合材料的简单合成,并研究了作为吸附剂的染料去除能力。以柠檬酸钠为还原剂,在Hummers法制备的氧化石墨烯薄片表面还原Au (III)离子形成金纳米颗粒。采用透射电镜(TEM)、傅里叶变换红外光谱(FT-IR)和x射线衍射(XRD)对纳米复合材料的合成进行了表征。考察了吸附量和接触时间对去除亚甲基蓝和甲基橙的影响。在最佳条件下,亚甲基蓝吸附剂用量为30 mg,接触时间为15 min,甲基橙吸附剂用量为30 mg,接触时间为25 min,对10 mL废水进行定量去除。拟二阶模型解释了动力学数据。由于氧化石墨烯/金纳米复合材料可以合理地重复使用,并且具有吸附性能,因此它倾向于作为一种适度的、选择性的吸附剂来处理废水。
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来源期刊
CiteScore
4.80
自引率
0.00%
发文量
256
期刊介绍: Biointerface Research in Applied Chemistry is an international and interdisciplinary research journal that focuses on all aspects of nanoscience, bioscience and applied chemistry. Submissions are solicited in all topical areas, ranging from basic aspects of the science materials to practical applications of such materials. With 6 issues per year, the first one published on the 15th of February of 2011, Biointerface Research in Applied Chemistry is an open-access journal, making all research results freely available online. The aim is to publish original papers, short communications as well as review papers highlighting interdisciplinary research, the potential applications of the molecules and materials in the bio-field. Our aim is to encourage scientists to publish their experimental and theoretical results in as much detail as possible.
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