Accuracy of surface strain measurements from transmission electron microscopy images of nanoparticles

Jacob Madsen, Pei Liu, Jakob B. Wagner, Thomas W. Hansen, Jakob Schiøtz
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引用次数: 18

Abstract

Strain analysis from high-resolution transmission electron microscopy (HRTEM) images offers a convenient tool for measuring strain in materials at the atomic scale. In this paper we present a theoretical study of the precision and accuracy of surface strain measurements directly from aberration-corrected HRTEM images. We examine the influence of defocus, crystal tilt and noise, and find that absolute errors of at least 1–2% strain should be expected. The model structures include surface relaxations determined using molecular dynamics, and we show that this is important for correctly evaluating the errors introduced by image aberrations.

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纳米颗粒透射电子显微镜图像表面应变测量的准确性
高分辨率透射电子显微镜(HRTEM)图像的应变分析为在原子尺度上测量材料的应变提供了一种方便的工具。本文对直接从像差校正的HRTEM图像测量表面应变的精度和准确性进行了理论研究。我们研究了离焦、晶体倾斜和噪声的影响,发现至少有1-2%的应变绝对误差应该是预期的。模型结构包括使用分子动力学确定的表面弛豫,我们表明这对于正确评估由像差引入的误差是重要的。
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Advanced Structural and Chemical Imaging
Advanced Structural and Chemical Imaging Medicine-Radiology, Nuclear Medicine and Imaging
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